Dicyclohexyliodoborane

Base Information

• Chemical Name: Dicyclohexyliodoborane
• CAS No.: 55382-85-9
• Molecular Formula: C12H22BI
• Molecular Weight: 304.022
• Hs Code.: 2931900090
• European Community (EC) Number: 687-074-3
• DSSTox Substance ID: DTXSID60404005
• Nikkaji Number: J519.581K
• Wikidata: Q82207944
• Mol file: 55382-85-9.mol

Synonyms:Dicyclohexyliodoborane;dicyclohexyl(iodo)borane;55382-85-9;Dicyclohexyliodoborane, 97%;SCHEMBL8953848;DTXSID60404005;AKOS015915720

Chemical Property of Dicyclohexyliodoborane

Chemical Property:

• Boiling Point: 68-69 °C
• Flash Point: 86 °F
• PSA: 0.00000
• Density: 1.325 g/mL at 25 °C(lit.)
• LogP: 5.08150
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 2
• Exact Mass: 304.08593
• Heavy Atom Count: 14
• Complexity: 142

Purity/Quality:

95% ^*data from raw suppliers

Dicyclohexyliodobora?ne ^*data from reagent suppliers

Safty Information:

• Hazard Codes: C,F,N,Xn
• Statements: 11-14-20/21/22-34-40-42/43-10-67-65-62-51/53-48/20-38
• Safety Statements: 16-26-27-36/37/39-45-23-62-61-36/37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: B(C1CCCCC1)(C2CCCCC2)I
• Uses: Reactant for:Preparation of vinyloxyboranes

Technology Process of Dicyclohexyliodoborane

There total 3 articles about Dicyclohexyliodoborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

bis(cyclohexanyl)borane (1568-65-6) → B-iododicyclohexylborane (55382-85-9)

Guidance literature:

With I₂; In hexane;

Reference yield:

tricyclohexylborane (1088-01-3) → B-iododicyclohexylborane (55382-85-9)

Guidance literature:

With iodine;

DOI:10.1002/zaac.19592990310

Reference yield:

tricyclohexylborane (1088-01-3) + iodine (7553-56-2,12190-71-5,8031-47-8) → B-iododicyclohexylborane (55382-85-9)

Guidance literature:

upstream raw materials:

tricyclohexylborane

bis(cyclohexanyl)borane

iodine

Downstream raw materials:

dicyclohexylhydroxyborane

dicyclohexylboron chloride

bis(dicyclohexylboryl)selenane

dimethyltin diiodide