3-(2-Carboxyphenyl)benzoic acid

Base Information

• Chemical Name: 3-(2-Carboxyphenyl)benzoic acid
• CAS No.: 606-75-7
• Molecular Formula: C14H10O4
• Molecular Weight: 242.231
• Hs Code.: 2917399090
• Mol file: 606-75-7.mol

Synonyms:3-(2-Carboxyphenyl)benzoic acid

Chemical Property of 3-(2-Carboxyphenyl)benzoic acid

Chemical Property:

• Melting Point: 215-216 °C(Solv: acetic acid (64-19-7))
• Boiling Point: 471.4±28.0 °C(Predicted)
• PKA: 3.76±0.36(Predicted)
• Flash Point: 253.035oC
• PSA: 74.60000
• Density: 1.347±0.06 g/cm3(Predicted)
• LogP: 2.75000

Purity/Quality:

98%min ^*data from raw suppliers

Biphenyl-2,3''-dicarboxylicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-Carboxyphenyl)benzoic acid

There total 13 articles about 3-(2-Carboxyphenyl)benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,3'-dimethyl-1,1'-biphenyl (611-43-8) → biphenyl-2,3'-dicarboxylic acid (606-75-7)

Guidance literature:

With potassium permanganate;

DOI:10.1021/ja01163a119

Reference yield:

ortho-tolylmagnesium bromide (932-31-0) → biphenyl-2,3'-dicarboxylic acid (606-75-7)

Guidance literature:

Multi-step reaction with 4 steps

1: diethyl ether

2: diethyl ether

3: palladium/charcoal

4: KMnO₄

With potassium permanganate; palladium on activated charcoal; diethyl ether;

DOI:10.1021/ja01163a119

Reference yield:

2'-methyl-5,6-dihydro-[1,1'-bi(phenyl)]-3(4H)-one (854726-99-1) → biphenyl-2,3'-dicarboxylic acid (606-75-7)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether

2: palladium/charcoal

3: KMnO₄

With potassium permanganate; palladium on activated charcoal; diethyl ether;

DOI:10.1021/ja01163a119

upstream raw materials:

2,3'-dimethyl-1,1'-biphenyl

9-oxo-9H-fluorene-3-carboxylic acid

9-oxo-9H-fluorene-1-carboxylic acid

carbon dioxide

Downstream raw materials:

biphenyl

9-fluorenone

carbon dioxide

9-oxo-9H-fluorene-1-carboxylic acid

Refernces