OOPORPYHRIN DIMETHYL ESTER

Base Information

• Chemical Name: OOPORPYHRIN DIMETHYL ESTER
• CAS No.: 6164-53-0
• Molecular Formula: C36H38N4O4
• Molecular Weight: 590.71
• Mol file: 6164-53-0.mol

Synonyms:OOPORPYHRIN DIMETHYL ESTER;PROTOPORPHYRIN DIMETHYL ESTER;PROTOPORPHYRIN IX METHYL ESTER;DIMETHYL-8,13-BIS(VINYL)-3,7,12,17-TETRAMETHYL-21H,23H-PORPHINE-2,18-DIPROPIONATE;Dimethyl-8,13-bi8(vinyl)-3,7,12,17-tetramethyl-21H,23H-porphine-2,18-dipropionate

Chemical Property of OOPORPYHRIN DIMETHYL ESTER

Chemical Property:

• Melting Point: 225-228 °C(lit.)
• PSA: 108.90000
• LogP: 4.21740

Purity/Quality:

99% ^*data from raw suppliers

Dimethyl-8,13-bi8(vinyl)-3,7,12,17-tetramethyl-21H,23Hporphine-2,18-dipropionate 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of OOPORPYHRIN DIMETHYL ESTER

There total 89 articles about OOPORPYHRIN DIMETHYL ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

methanol (67-56-1) + hemin (13496-05-4,16009-13-5) → 3,3'-(3,7,12,17-tetramethyl-8,13-divinyl-21H,23H-porphine-2,18-diyl)-bis-propionic acid dimethyl ester (5522-66-7,6164-53-0)

Guidance literature:

With pyridine; diammonium iron(II) sulfate hexahydrate; acetyl chloride; In dichloromethane; for 1h; Cooling;

DOI:10.1016/j.mencom.2020.03.027

Reference yield: 98.0%

methanol (67-56-1) + protoporphyrin IX (553-12-8) → 3,3'-(3,7,12,17-tetramethyl-8,13-divinyl-21H,23H-porphine-2,18-diyl)-bis-propionic acid dimethyl ester (5522-66-7,6164-53-0)

Guidance literature:

at 20 ℃; for 6h;

DOI:10.1142/S1088424615500650

Reference yield: 79.0%

protoporphyrin IX (553-12-8) → 3,3'-(3,7,12,17-tetramethyl-8,13-divinyl-21H,23H-porphine-2,18-diyl)-bis-propionic acid dimethyl ester (5522-66-7,6164-53-0)

Guidance literature:

With sulfuric acid; In methanol; for 12h; Darkness;

DOI:10.1016/j.dyepig.2017.06.011

upstream raw materials:

diazomethane

protoporphyrin IX

hematoporphyrin-dimethyl ester

protoporphyrin

Downstream raw materials:

diacetyldeuteroporphyrin IX dimethyl ester

dimethyl 3,8-bis(1-methoxyethyl)-2,7,12,18-tetramethylporphyrin-13,17dipropanoate

3-{(5Z,10Z,14Z,19Z)-18-(2-Methoxycarbonyl-ethyl)-12-(1-methoxy-ethyl)-7-[1-(4-methoxy-phenyl)-ethyl]-3,8,13,17-tetramethyl-porphyrin-2-yl}-propionic acid methyl ester

3-{(5Z,10Z,14Z,19Z)-18-(2-Methoxycarbonyl-ethyl)-12-(1-methoxy-ethyl)-7-[1-(2-methoxy-phenyl)-ethyl]-3,8,13,17-tetramethyl-porphyrin-2-yl}-propionic acid methyl ester

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