Ribonic acid, 2-amino-2,3,5-trideoxy-3-methyl-, gamma-lactone (9CI)

Base Information

• Chemical Name: Ribonic acid, 2-amino-2,3,5-trideoxy-3-methyl-, gamma-lactone (9CI)
• CAS No.: 681230-42-2
• Molecular Formula: C6H11NO2
• Molecular Weight: 129.16
• Mol file: 681230-42-2.mol

Synonyms:Ribonic acid, 2-amino-2,3,5-trideoxy-3-methyl-, gamma-lactone (9CI)

Chemical Property of Ribonic acid, 2-amino-2,3,5-trideoxy-3-methyl-, gamma-lactone (9CI)

Chemical Property:

• Melting Point: 240-245 °C
• Boiling Point: 245.6±33.0 °C(Predicted)
• PKA: 7.93±0.60(Predicted)
• Density: 1.043±0.06 g/cm3(Predicted)

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Ribonic acid, 2-amino-2,3,5-trideoxy-3-methyl-, gamma-lactone (9CI)

There total 48 articles about Ribonic acid, 2-amino-2,3,5-trideoxy-3-methyl-, gamma-lactone (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

3-(dibenzylamino)-4,5-dimethyldihydrofuran-2(3H)-one → 3-amino-4,5-dimethyldihydrofuran-2(3H)-one (168610-73-9,681230-42-2,695148-12-0,697797-11-8)

Guidance literature:

With 10 wt% Pd(OH)2 on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 1h;

Reference yield: 99.0%

(3R,4R,5S)-3-(dibenzylamino)-4,5-dimethyldihydrofuran-2(3H)-one → (3R,4R,5S)-3-amino-4,5-dimethyldihydrofuran-2(3H)-one (363172-09-2,168610-73-9,681230-42-2,695148-12-0,697797-11-8)

Guidance literature:

With hydrogen; palladium(II) hydroxide; In ethyl acetate; at 20 ℃; for 18h;

DOI:10.1074/jbc.M115.672097

Reference yield: 99.0%

(3S,4S,5R)-3-(dibenzylamino)-4,5-dimethyldihydrofuran-2(3H)-one → (3S,4S,5R)-3-amino-4,5-dimethyldihydrofuran-2(3H)-one (71392-28-4,168610-73-9,681230-42-2,695148-12-0,697797-11-8)

Guidance literature:

With 10 wt% Pd(OH)2 on carbon; hydrogen; In ethyl acetate; at 20 ℃; for 18h; under 760.051 Torr;

DOI:10.1039/d0ob01722a

upstream raw materials:

L-isoleucine

(2S,3R,4R)-2-amino-4-hydroxy-3-methyl-pentanoic acid

ethyl (2S,3R)-2-amino-3-methyl-4-oxopentanoate

(2S,3S)-ethyl 2-(p-methoxyphenylamino)-3-methyl-4-oxo-pentanoate

Downstream raw materials:

(-)-funebrine

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