Benzenemethanamine, alpha-ethenyl-3-fluoro-, (alphaS)- (9CI)

Base Information

Chemical Name:Benzenemethanamine, alpha-ethenyl-3-fluoro-, (alphaS)- (9CI)
CAS No.:688362-63-2
Molecular Formula:C9H10FN
Molecular Weight:151.1808032
Hs Code.:
Mol file:688362-63-2.mol

Synonyms:Benzenemethanamine, alpha-ethenyl-3-fluoro-, (alphaS)- (9CI)

Suppliers and Price of Benzenemethanamine, alpha-ethenyl-3-fluoro-, (alphaS)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzenemethanamine, alpha-ethenyl-3-fluoro-, (alphaS)- (9CI)

Chemical Property:

Purity/Quality:: 99%+ ^*data from raw suppliers

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Technology Process of Benzenemethanamine, alpha-ethenyl-3-fluoro-, (alphaS)- (9CI)

There total 5 articles about Benzenemethanamine, alpha-ethenyl-3-fluoro-, (alphaS)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 688362-49-4
(+/-)-N-1-acetyl-1-(3-fluorophenyl)-2-propenylamine

: 688362-56-3,688362-63-2
(+/-)-1-(3-fluorophenyl)-2-propenylamine

Guidance literature:: With hydrogenchloride; at 90 ℃; for 18h;
DOI:10.1016/j.tetasy.2004.01.035

Reference yield:

: 226698-92-6
(+/-)-N-[1-(3-fluorophenyl)-2-propynyl]acetamide

: 688362-56-3,688362-63-2
(+/-)-1-(3-fluorophenyl)-2-propenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / H₂ / Lindlar catalyst / dimethylformamide; ethane-1,2-diamine / 3 h / 20 °C / 760 Torr

2: 55 percent / aq. HCl / 18 h / 90 °C

With hydrogenchloride; hydrogen; Lindlar's catalyst; In ethylenediamine; N,N-dimethyl-formamide;
DOI:10.1016/j.tetasy.2004.01.035

Reference yield:

: 141-78-6
ethyl acetate

: 688362-56-3,688362-63-2
(+/-)-1-(3-fluorophenyl)-2-propenylamine

: 688362-63-2
(R)-1-(3-fluorophenyl)-2-propenylamine

: 688362-63-2
(S)-1-(3-fluorophenyl)-2-propenylamine

: (S)-N-1-acetyl-1-(3-fluorophenyl)-2-propenylamine

: (R)-N-1-acetyl-1-(3-fluorophenyl)-2-propenylamine

Guidance literature:: With Candida antarctica lipase; In diethyl ether; at 20 ℃; for 168h; Title compound not separated from byproducts;
DOI:10.1016/j.tetasy.2004.01.035