4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT

Base Information

Chemical Name:4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT
CAS No.:618900-67-7
Molecular Formula:C11H17FLiNO4
Molecular Weight:253.2
Hs Code.:
Mol file:618900-67-7.mol

Synonyms:4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT

Suppliers and Price of 4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT 95.00%
1G
$ 854.70

Total 3 raw suppliers

Chemical Property of 4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT

Chemical Property:

PSA：69.67000
LogP:0.41340

Purity/Quality:

98%min ^*data from raw suppliers

4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT

There total 2 articles about 4-FLUORO-1,4-PIPERIDINEDICHARBOXYLIC ACID,1(1,1-DIMETHYLETHYL)ESTER, LITHIUM SALT which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 416852-82-9
4-fluoropiperidine-1,4-dicarboxylic acid 1-tert-butyl ester 4-ethyl ester

: 618900-67-7
C₁₁H₁₇FNO₄^(1-)*Li⁽¹⁺⁾

Guidance literature:: With lithium hydroxide; water; In tetrahydrofuran; methanol; at 45 ℃; for 6h;

Reference yield:

: 142851-03-4
1-tert-butyl 4-ethyl piperidine-1,4-dicarboxylate

: 618900-67-7
C₁₁H₁₇FNO₄^(1-)*Li⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane; ethylbenzene / 0.5 h / 0 °C

1.2: 18.5 h / 0 - 20 °C

2.1: lithium hydroxide; water / tetrahydrofuran; methanol / 6 h / 45 °C

With lithium hydroxide; water; lithium diisopropyl amide; In tetrahydrofuran; methanol; n-heptane; ethylbenzene;