4-[2-(DIMETHYLAMINO)ETHYLAMINOSULFONYL]-7-CHLORO-2,1,3-BENZOXADIAZOLE

Base Information

• Chemical Name: 4-[2-(DIMETHYLAMINO)ETHYLAMINOSULFONYL]-7-CHLORO-2,1,3-BENZOXADIAZOLE
• CAS No.: 664985-43-7
• Molecular Formula: C10H13ClN4O3S
• Molecular Weight: 304.75
• Hs Code.: 2935009090
• Mol file: 664985-43-7.mol

Synonyms:DAABD-CL;4-[2-(DIMETHYLAMINO)ETHYLAMINOSULFONYL]-7-CHLORO-2,1,3-BENZOXADIAZOLE;DAABD-Cl [=4-[2-(Dimethylamino)ethylaminosulfonyl]-7-chloro-2,1,3-benzoxadiazole] [for Proteome Analysis]

Chemical Property of 4-[2-(DIMETHYLAMINO)ETHYLAMINOSULFONYL]-7-CHLORO-2,1,3-BENZOXADIAZOLE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.595
• Boiling Point: 436.683°C at 760 mmHg
• Flash Point: 217.898°C
• PSA: 96.71000
• Density: 1.437g/cm³
• LogP: 2.18780
• Storage Temp.: Refrigerator
• Solubility.: DMSO (Slightly), Methanol (Slightly)

Purity/Quality:

97% ^*data from raw suppliers

DAABD-Cl ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-[2-(DIMETHYLAMINO)ETHYLAMINOSULFONYL]-7-CHLORO-2,1,3-BENZOXADIAZOLE

There total 2 articles about 4-[2-(DIMETHYLAMINO)ETHYLAMINOSULFONYL]-7-CHLORO-2,1,3-BENZOXADIAZOLE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.4%

7-chlorobenzo[c][1,2,5]oxadiazole-4-sulfonic acid chloride (142246-48-8) + N,N-dimethylethylenediamine (108-00-9) → 7-chloro-N-[2-(dimethylamino)ethyl]-2,1,3-benzoxadiazole-4-sulfonamide (664985-43-7)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 0.166667h;

DOI:10.1021/ac034840i

Reference yield:

→ 7-chloro-N-[2-(dimethylamino)ethyl]-2,1,3-benzoxadiazole-4-sulfonamide (664985-43-7)

Guidance literature:

With triethylamine;

upstream raw materials:

7-chlorobenzo[c][1,2,5]oxadiazole-4-sulfonic acid chloride

N,N-dimethylethylenediamine