4,4,4-Trifluoro-1-(1-naphthyl)butane-1,3-dione

Base Information

Chemical Name:4,4,4-Trifluoro-1-(1-naphthyl)butane-1,3-dione
CAS No.:7639-68-1
Molecular Formula:C14 H9 F3 O2
Molecular Weight:266.219
Hs Code.:2914700090
DSSTox Substance ID:DTXSID20997761
Nikkaji Number:J922.136K
Wikidata:Q82990045
Mol file:7639-68-1.mol

Synonyms:7639-68-1;4,4,4-trifluoro-1-(1-naphthyl)butane-1,3-dione;4,4,4-Trifluoro-1-naphthalen-1-yl-butane-1,3-dione;4,4,4-trifluoro-1-(naphthalen-1-yl)butane-1,3-dione;4,4,4-trifluoro-1-naphthalen-1-ylbutane-1,3-dione;4,4,4-Trifluoro-1-(1-naphthalenyl)-1,3-butanedione;naphthoyltrifluoroacetone;alpha-Naphthoyltrifluoroacetone;SCHEMBL710254;DTXSID20997761;UYQMAGRFYJIJOQ-UHFFFAOYSA-N;BBL038788;MFCD00429745;STK312556;AKOS000210408;CS-0215209;4,4,4-trifluoro-1-naphthyl-1,3-butanedione;C78448;EN300-228439;A923196

Suppliers and Price of 4,4,4-Trifluoro-1-(1-naphthyl)butane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Oakwood
4,4,4-Trifluoro-1-naphthalen-1-yl-butane-1,3-dione
100mg
$ 85.00

Chemenu
4,4,4-trifluoro-1-(naphthalen-1-yl)butane-1,3-dione 95%
10g
$ 342.00

Arctom
4,4,4-Trifluoro-1-naphthalen-1-yl-butane-1,3-dione 97%
1g
$ 255.00

Acrotein
4,4,4-Trifluoro-1-(1-naphthalenyl)-1,3-butanedione 97%
0.5g
$ 121.00

Total 8 raw suppliers

Chemical Property of 4,4,4-Trifluoro-1-(1-naphthyl)butane-1,3-dione

Chemical Property:

Melting Point:45-46 °C
Boiling Point:350.7±37.0 °C(Predicted)
PKA:7.70±0.50(Predicted)
PSA：34.14000
Density:1.320±0.06 g/cm3(Predicted)
LogP:3.54400
XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:266.05546401
Heavy Atom Count:19
Complexity:362

Purity/Quality:

97% ^*data from raw suppliers

4,4,4-Trifluoro-1-naphthalen-1-yl-butane-1,3-dione ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C2C(=C1)C=CC=C2C(=O)CC(=O)C(F)(F)F

Technology Process of 4,4,4-Trifluoro-1-(1-naphthyl)butane-1,3-dione

There total 1 articles about 4,4,4-Trifluoro-1-(1-naphthyl)butane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 941-98-0
1'-naphthacetophenone

: 383-63-1
ethyl trifluoroacetate,

: 7639-68-1
4,4,4-trifluoro-1-(1-naphthyl)-1,3-butanedione

Guidance literature:: With methanol; sodium hydride; In tetrahydrofuran;
DOI:10.1016/j.dyepig.2021.109701

Reference yield: 83.0%

: 7639-68-1
4,4,4-trifluoro-1-(1-naphthyl)-1,3-butanedione

: 459-57-4
4-fluorobenzaldehyde

: 17356-08-0
thiourea

: (6-(4-fluorophenyl)-4-hydroxy-2-thioxo-4-(trifluoromethyl)hexahydropyrimidin-5-yl)(naphthalen-1-yl)methanone

Guidance literature:: With polyphosphoric ester; In tetrahydrofuran; for 24h; Reflux;
DOI:10.1016/j.bmcl.2010.12.022

Reference yield:

: 7639-68-1
4,4,4-trifluoro-1-(1-naphthyl)-1,3-butanedione

: 100-16-3
4-nitrophenylhydrazone

: 1177469-53-2
4-(5-naphthalen-1-yl-3-trifluoromethyl-pyrazol-1-yl)-phenylamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / ethanol / Reflux

2: platinum(IV) oxide; hydrogen / ethanol

With hydrogenchloride; platinum(IV) oxide; hydrogen; In ethanol;
DOI:10.1016/j.bmc.2012.06.018