Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI)

Base Information

• Chemical Name: Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI)
• CAS No.: 68897-45-0
• Molecular Formula: C8H18N4
• Molecular Weight: 170.258
• Mol file: 68897-45-0.mol

Synonyms:1,1,2,2,3,3-Hexamethylguanidiniumcyanid;N,N,N',N',N'',N''-Hexamethylguanidiniumcyanid;Hexamethylguanidinium cyanide;

Chemical Property of Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI)

Chemical Property:

• PSA: 33.28000
• LogP: -0.16592

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI)

There total 3 articles about Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

trimethylsilyl cyanide (7677-24-9) + hexamethylguanidinium methylcarbonate (1283076-09-4) → N,N,N',N',N'',N''-Hexamethylguanidiniumcyanid (68897-45-0)

Guidance literature:

In acetonitrile; at 0 - 20 ℃; for 1.25h; Schlenk technique;

DOI:10.1021/acs.inorgchem.5b01665

Reference yield: 91.0%

1,1,2,2,3,3-Hexamethylguanidinium-tetrafluoroborat → N,N,N',N',N'',N''-Hexamethylguanidiniumcyanid (68897-45-0)

Guidance literature:

With sodium cyanide; In methanol; at 10 - 15 ℃;

Reference yield: 32.7%

Acetyl cyanide (631-57-2) + N,N,N',N',N'',N''-Hexamethyl(methoxy)methantriamin (58392-99-7) → N,N,N',N',N'',N''-Hexamethylguanidiniumcyanid (68897-45-0)

Guidance literature:

In diethyl ether; for 1.5h; Ambient temperature;

upstream raw materials:

Acetyl cyanide

N,N,N',N',N'',N''-Hexamethyl(methoxy)methantriamin

trimethylsilyl cyanide

hexamethylguanidinium methylcarbonate

Downstream raw materials:

hexanedinitrile

1,1,2,2,3,3-Hexamethylguanidiniumbromid

pentanonitrile

propiononitrile

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 68897-45-0 Methanaminium, N-[bis(dimethylamino)methylene]-N-methyl-, cyanide (9CI)

Send

Send

Metric Ton KG G Pound L ML

Send

Send