(Z)-2-(5-AMINO-1,2,4-THIADIAZOL-3-YL)-2-METHOXYIMINO ACETIC ACID

Base Information

Chemical Name:(Z)-2-(5-AMINO-1,2,4-THIADIAZOL-3-YL)-2-METHOXYIMINO ACETIC ACID
CAS No.:68786-47-0
Molecular Formula:C43H33 N3 O3 S
Molecular Weight:671.819
Hs Code.:
Mol file:68786-47-0.mol

Synonyms:4-Thiazoleaceticacid, a-[(triphenylmethoxy)imino]-2-[(triphenylmethyl)amino]-,(Z)-; (Z)-2-(Trityloxyimino)-2-[2-(tritylamino)thiazol-4-yl]acetic acid;(Z)-2-[2-(Tritylamino)thiazol-4-yl]-2-(trityloxyimino)acetic acid

Suppliers and Price of (Z)-2-(5-AMINO-1,2,4-THIADIAZOL-3-YL)-2-METHOXYIMINO ACETIC ACID

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(Z)-2-(2-TRITYLAMINOTHIAZOL-4-YL)-2-TRITYLOXY IMINOACETIC ACID 95.00%
5G
$ 1249.13

Total 11 raw suppliers

Chemical Property of (Z)-2-(5-AMINO-1,2,4-THIADIAZOL-3-YL)-2-METHOXYIMINO ACETIC ACID

Chemical Property:

Vapor Pressure:2.08E-29mmHg at 25°C
Boiling Point:832.8oC at 760 mmHg
Flash Point:457.5oC
PSA：112.05000
Density:1.19g/cm3
LogP:9.41750

Purity/Quality:

98% ^*data from raw suppliers

(Z)-2-(2-TRITYLAMINOTHIAZOL-4-YL)-2-TRITYLOXY IMINOACETIC ACID 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses Intermediate in the preparation of Cefdinir (C242670).

Technology Process of (Z)-2-(5-AMINO-1,2,4-THIADIAZOL-3-YL)-2-METHOXYIMINO ACETIC ACID

There total 5 articles about (Z)-2-(5-AMINO-1,2,4-THIADIAZOL-3-YL)-2-METHOXYIMINO ACETIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 69689-86-7
ethyl 2-(2-tritylaminothiazol-4-yl)-(Z)-2-(tritylhydroxyimino)acetate

: 68786-47-0
(Z)-2-(trityloxyimino)-2-(2-tritylamino-4-thiazolyl)acetic acid

Guidance literature:: With water; sodium hydroxide; In 1,4-dioxane; at 100 ℃;

Reference yield:

: 64485-82-1
(Z)-ethyl 2-(2-aminothiazol-4-yl)-2-hydroxyiminoacetate

: 68786-47-0
(Z)-2-(trityloxyimino)-2-(2-tritylamino-4-thiazolyl)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CHCl₃ / 2 h / 20 °C

2: aq. NaOH / dioxane / 2 h / Heating

With sodium hydroxide; triethylamine; In 1,4-dioxane; chloroform;
DOI:10.1016/0040-4020(78)89034-6