Li[Fe2Cp2(μ-PPh2)(CO)2]

Base Information

Chemical Name:Li[Fe2Cp2(μ-PPh2)(CO)2]
CAS No.:778583-08-7
Molecular Formula:C₂₄H₂₀Fe₂O₂P*Li
Molecular Weight:490.03
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Li[Fe2Cp2(μ-PPh2)(CO)2]

Chemical Property:

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Technology Process of Li[Fe2Cp2(μ-PPh2)(CO)2]

There total 1 articles about Li[Fe2Cp2(μ-PPh2)(CO)2] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-72-8,29786-93-4
n-butyllithium

: 640282-25-3,106323-09-5,779357-74-3
cis-[Fe2(η5-C5H5)2(μ-H)(μ-PPh2)(CO)2]

: 778583-08-7
Li[Fe2Cp2(μ-PPh2)(CO)2]

Guidance literature:: In tetrahydrofuran; Petroleum ether; (N2); addn. of a soln. of lithium compd. in petroleum ether to a soln. of iron complex in THF at room temp., stirring for 5 min; not isolated, detected by NMR and IR;
DOI:10.1021/om049574t

Reference yield: 75.0%

: 33659-45-9
[AuCl(PiPr₃)]

: 778583-08-7
Li[Fe2Cp2(μ-PPh2)(CO)2]

: 778583-10-1,779357-75-4
[AuFe2Cp2(μ-PPh2)(CO)2(P(i)Pr3)]

Guidance literature:: In tetrahydrofuran; (N2); addn. of gold complex to a soln. of iron complex in THF, stirring at room temp. for 5 min; evapn., extn. with CH2Cl2/petroleum ether 1:1, column chromy. (alumina, 15°C, petroleum ether, then CH2Cl2/petroleum ether 1:1), evapn.; elem. anal.;
DOI:10.1021/om049574t

Reference yield: 66.0%

: 778583-08-7
Li[Fe2Cp2(μ-PPh2)(CO)2]

: 74-88-4
methyl iodide

: 778583-13-4
[Fe2Cp2(μ-PPh2)(Me)(μ-CO)(CO)]

Guidance literature:: In tetrahydrofuran; (N2); addn. of excess of CH3I to a soln. of iron complex in THF, stirring at room temp. for 5 min; evapn., extn. with toluene, filtration, evapn. washing with petroleum ether;
DOI:10.1021/om049574t