Technology Process of C29H30N2S
There total 6 articles about C29H30N2S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate;
at 20 ℃;
for 1h;
Inert atmosphere;
DOI:10.1021/jo200675j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: potassium iodate; acetic acid; potassium iodide / 0.17 h / Reflux
2: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C
3: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran; water / 6 h / Reflux; Inert atmosphere
4: ethanol; dichloromethane / 8 h / Reflux; Inert atmosphere
5: sodium tetrahydroborate / 1 h / 20 °C / Inert atmosphere
With
potassium iodate; sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); sodium hydride; potassium carbonate; acetic acid; potassium iodide;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo200675j
- Guidance literature:
-
Multi-step reaction with 4 steps
1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C
2: tetrakis(triphenylphosphine) palladium(0); potassium carbonate / tetrahydrofuran; water / 6 h / Reflux; Inert atmosphere
3: ethanol; dichloromethane / 8 h / Reflux; Inert atmosphere
4: sodium tetrahydroborate / 1 h / 20 °C / Inert atmosphere
With
sodium tetrahydroborate; tetrakis(triphenylphosphine) palladium(0); sodium hydride; potassium carbonate;
In
tetrahydrofuran; ethanol; dichloromethane; water; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/jo200675j
