1-[2-(4-Methoxyphenyl)vinyl]-2-vinylbenzene

Base Information

Chemical Name:1-[2-(4-Methoxyphenyl)vinyl]-2-vinylbenzene
CAS No.:207619-53-2
Molecular Formula:C₁₇H₁₆O
Molecular Weight:236.313
Hs Code.:
DSSTox Substance ID:DTXSID501217526

Synonyms:1-[2-(4-methoxyphenyl)vinyl]-2-vinylbenzene;1-ethenyl-2-[(E)-2-(4-methoxyphenyl)ethenyl]benzene;DTXSID501217526;AB-131/42301510;1-Ethenyl-2-[(1E)-2-(4-methoxyphenyl)ethenyl]benzene;207619-53-2

Suppliers and Price of 1-[2-(4-Methoxyphenyl)vinyl]-2-vinylbenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[2-(4-Methoxyphenyl)vinyl]-2-vinylbenzene

Chemical Property:

Boiling Point:384.9±27.0 °C(Predicted)
Density:1.061±0.06 g/cm3(Predicted)
XLogP3:4.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:4
Exact Mass:236.120115130
Heavy Atom Count:18
Complexity:273

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1=CC=C(C=C1)C=CC2=CC=CC=C2C=C
Isomeric SMILES:COC1=CC=C(C=C1)/C=C/C2=CC=CC=C2C=C

Technology Process of 1-[2-(4-Methoxyphenyl)vinyl]-2-vinylbenzene

There total 3 articles about 1-[2-(4-Methoxyphenyl)vinyl]-2-vinylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1220094-19-8
(E)-1-formyl-2-[2-(4-methoxyphenyl)ethenyl]benzene

: 1779-49-3
Methyltriphenylphosphonium bromide

: 207619-53-2
(E)-1-(4-methoxystyryl)-2-vinylbenzene

Guidance literature:: With sodium hydride; In tetrahydrofuran; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1021/acs.joc.9b00939

Reference yield: 34.0%

: 637-69-4,24936-44-5
4-Methoxystyrene

: 2039-88-5
2-bromostyrene

: 207619-53-2
(E)-1-(4-methoxystyryl)-2-vinylbenzene

: 2-(4'-methoxyphenyl)-3-methyleneindane

Guidance literature:: With palladium diacetate; tetrabutylammomium bromide; potassium hydrogencarbonate; lithium chloride; In various solvent(s); at 100 ℃; for 48h; Title compound not separated from byproducts;

Reference yield:

: 6630-33-7
ortho-bromobenzaldehyde

: 207619-53-2
(E)-1-(4-methoxystyryl)-2-vinylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / NaH, DMSO / tetrahydrofuran / 1 h / 80 °C

2: 17 percent / Pd(OAc)2, LiCl, KHCO₃, Bu₄NBr / various solvent(s) / 48 h / 100 °C

With palladium diacetate; tetrabutylammomium bromide; sodium hydride; potassium hydrogencarbonate; dimethyl sulfoxide; lithium chloride; In tetrahydrofuran;