C₃₀H₂₅BF₂N₂O₃

Base Information

• Chemical Name: C₃₀H₂₅BF₂N₂O₃
• CAS No.: 1567408-63-2
• Molecular Formula: C₃₀H₂₅BF₂N₂O₃
• Molecular Weight: 510.348
• Mol file: 1567408-63-2.mol

Synonyms:

Chemical Property of C₃₀H₂₅BF₂N₂O₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₀H₂₅BF₂N₂O₃

There total 4 articles about C₃₀H₂₅BF₂N₂O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → C30H25BF2N2O3 (1567408-63-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: trifluoroacetic acid / 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 20 °C

2.2: Reflux

3.1: N-Bromosuccinimide / tetrahydrofuran / Cooling with ice

4.1: potassium carbonate; palladium diacetate; tris-(o-tolyl)phosphine / water; 1,2-dimethoxyethane / Reflux

With N-Bromosuccinimide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,2-dimethoxyethane; water;

DOI:10.1039/c3tb21547d

Reference yield:

5-(4-methoxyphenyl)dipyrromethane (176446-62-1) → C30H25BF2N2O3 (1567408-63-2)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / tetrahydrofuran / 20 °C

1.2: Reflux

2.1: N-Bromosuccinimide / tetrahydrofuran / Cooling with ice

3.1: potassium carbonate; palladium diacetate; tris-(o-tolyl)phosphine / water; 1,2-dimethoxyethane / Reflux

With N-Bromosuccinimide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; 1,2-dimethoxyethane; water;

DOI:10.1039/c3tb21547d

Reference yield:

1-bromo-4-methoxy-benzene (104-92-7) → C30H25BF2N2O3 (1567408-63-2)

Guidance literature:

Multi-step reaction with 2 steps

1: bis-triphenylphosphine-palladium(II) chloride; triethylamine / 1,4-dioxane / Reflux

2: potassium carbonate; palladium diacetate; tris-(o-tolyl)phosphine / water; 1,2-dimethoxyethane / Reflux

With bis-triphenylphosphine-palladium(II) chloride; palladium diacetate; potassium carbonate; triethylamine; tris-(o-tolyl)phosphine; In 1,4-dioxane; 1,2-dimethoxyethane; water;

DOI:10.1039/c3tb21547d

upstream raw materials:

4-methoxy-benzaldehyde

5-(4-methoxyphenyl)dipyrromethane

C₁₆H₁₁BBr₂F₂N₂O

2-(4-methoxyphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane