[2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2)

Base Information

Chemical Name:[2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2)
CAS No.:359445-51-5
Molecular Formula:C₃₄H₂₉NO₃Ru
Molecular Weight:600.679
Hs Code.:

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Chemical Property of [2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2)

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Technology Process of [2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2)

There total 2 articles about [2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 12321-08-3
tricarbonyl(2,3,4,5-tetraphenylcyclopentadienone)ruthenium

: 75-31-0
isopropylamine

: 359445-51-5
[2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2)

Guidance literature:: In water; toluene; 2 equiv. of ligand added to soln. of Ru complex in toluene-H2O; stirred for 2 h; concd. under vac.; extd. with CH2Cl2; chromd. (silica gel, CH2Cl2-ethyl acetate);
DOI:10.1021/om020097t

Reference yield: 44.0%

: 12321-08-3
tricarbonyl(2,3,4,5-tetraphenylcyclopentadienone)ruthenium

: ammonium chloride

: 67-64-1
acetone

: 359445-51-5
[2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2)

Guidance literature:: With sodium carbonate; In water; acetone; satd. aq. soln. of Na2CO3 added to soln. of Ru complex in acetone at ambient temp.; stirred for 1 h; cooled to 0°C; acidified by additionof satd. aq. soln. of NH4Cl; concd. under vac.; extd. with CH2Cl2; chromd. (silica gel, CH2Cl2-ethyl acetate); elem. anal.;
DOI:10.1021/om020097t

Reference yield:

: 359445-51-5
[2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(H2NCHMe2)

: 7789-20-0
water-d2

: [2,3,4,5-Ph4(η4-C4CO)](CO)2Ru(D2NCHMe2)

Guidance literature:: In chloroform-d1; D2O added to soln. of Ru complex in CDCl3; heated at 80°C; detd. by (1)H NMR spectra;
DOI:10.1021/om020097t