C₂₅H₂₆N₄O₃

Base Information

Chemical Name:C₂₅H₂₆N₄O₃
CAS No.:1333418-82-8
Molecular Formula:C₂₅H₂₆N₄O₃
Molecular Weight:430.506
Hs Code.:

C<sub>25</sub>H<sub>26</sub>N<sub>4</sub>O<sub>3</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₆N₄O₃

Chemical Property:

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Technology Process of C₂₅H₂₆N₄O₃

There total 3 articles about C₂₅H₂₆N₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1333418-81-7
1-amino-4-[4-(ethoxycarbonyl)-(E)-phenylazo]-2,3,5,6-tetramethylbenzene

: 108-95-2,27073-41-2
phenol

: 1333418-82-8
C₂₅H₂₆N₄O₃

Guidance literature:: 1-amino-4-[4-(ethoxycarbonyl)-(E)-phenylazo]-2,3,5,6-tetramethylbenzene; With nitrosylsulfuric acid; In sulfuric acid; acetic acid; propionic acid; at 0 - 5 ℃;

phenol; With sodium hydroxide; In sulfuric acid; water; acetic acid; propionic acid; at 20 ℃; Cooling with ice;
DOI:10.1021/om200479g

Reference yield:

: 7476-79-1
4-nitrosobenzoic acid ethyl ester

: 1333418-82-8
C₂₅H₂₆N₄O₃

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / toluene / 24 h / Reflux

2.1: nitrosylsulfuric acid / sulfuric acid; acetic acid; propionic acid / 0 - 5 °C

2.2: 20 °C / Cooling with ice

With nitrosylsulfuric acid; acetic acid; In sulfuric acid; acetic acid; propionic acid; toluene;
DOI:10.1021/om200479g

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 1333418-82-8
C₂₅H₂₆N₄O₃

Guidance literature:: Multi-step reaction with 3 steps

1.1: Oxone / dichloromethane; water / 1 h / Inert atmosphere

2.1: acetic acid / toluene / 24 h / Reflux

3.1: nitrosylsulfuric acid / sulfuric acid; acetic acid; propionic acid / 0 - 5 °C

3.2: 20 °C / Cooling with ice

With Oxone; nitrosylsulfuric acid; acetic acid; In dichloromethane; sulfuric acid; water; acetic acid; propionic acid; toluene;
DOI:10.1021/om200479g