C₄₈H₅₂N₈O₁₁S

Base Information

Chemical Name:C₄₈H₅₂N₈O₁₁S
CAS No.:1380110-89-3
Molecular Formula:C₄₈H₅₂N₈O₁₁S
Molecular Weight:949.054
Hs Code.:

C<sub>48</sub>H<sub>52</sub>N<sub>8</sub>O<sub>11</sub>S

Synonyms:

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Chemical Property of C₄₈H₅₂N₈O₁₁S

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Technology Process of C₄₈H₅₂N₈O₁₁S

There total 20 articles about C₄₈H₅₂N₈O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.8%

: 1380110-88-2
C₂₃H₂₇N₃O₇S

: 1380110-42-8
1-(((2R,3S)-3-amino-4-oxoazetidin-2-yl)-methyl)-3-((1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridin-2-yl)methyl)urea trifluoroacetic acid salt

: 1380110-89-3
C₄₈H₅₂N₈O₁₁S

Guidance literature:: C₂₃H₂₇N₃O₇S; With sodium hydrogencarbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

1-(((2R,3S)-3-amino-4-oxoazetidin-2-yl)-methyl)-3-((1,5-bis(benzyloxy)-4-oxo-1,4-dihydropyridin-2-yl)methyl)urea trifluoroacetic acid salt; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jm400560z

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1380110-89-3
C₄₈H₅₂N₈O₁₁S

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydroxide / methanol; water / 0.17 h / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: potassium iodide / N,N-dimethyl-formamide / 20 °C

6.1: hydrazine hydrate / ethanol / 1 h / Reflux

7.1: ethyl acetate / 2 h / 50 °C

8.1: potassium phosphate / dichloromethane; water / 1 h / 22 °C

9.1: potassium phosphate; dipotassium peroxodisulfate / acetonitrile; water / 1.5 h / 75 °C

10.1: trifluoroacetic acid / 3 h / 0 °C

11.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

11.2: 20 °C / Inert atmosphere

With potassium phosphate; dipotassium peroxodisulfate; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; hydrazine hydrate; triethylamine; trifluoroacetic acid; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400560z

Reference yield:

: 100-39-0
benzyl bromide

: 1380110-89-3
C₄₈H₅₂N₈O₁₁S

Guidance literature:: Multi-step reaction with 11 steps

1.1: sodium hydroxide / methanol; water / 0.17 h / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: potassium iodide / N,N-dimethyl-formamide / 20 °C

6.1: hydrazine hydrate / ethanol / 1 h / Reflux

7.1: ethyl acetate / 2 h / 50 °C

8.1: potassium phosphate / dichloromethane; water / 1 h / 22 °C

9.1: potassium phosphate; dipotassium peroxodisulfate / acetonitrile; water / 1.5 h / 75 °C

10.1: trifluoroacetic acid / 3 h / 0 °C

11.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; sodium hydrogencarbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

11.2: 20 °C / Inert atmosphere

With potassium phosphate; dipotassium peroxodisulfate; hydroxylamine hydrochloride; sodium acetate; sodium hydrogencarbonate; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; hydrazine hydrate; triethylamine; trifluoroacetic acid; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm400560z