(AuCl)2[(μ-PhN(P(OC6H4OMe-o)2)]

Base Information

Chemical Name:(AuCl)2[(μ-PhN(P(OC6H4OMe-o)2)]
CAS No.:1013639-52-5
Molecular Formula:C₃₄H₃₃Au₂Cl₂NO₈P₂
Molecular Weight:1110.42
Hs Code.:

Synonyms:

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Chemical Property of (AuCl)2[(μ-PhN(P(OC6H4OMe-o)2)]

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Technology Process of (AuCl)2[(μ-PhN(P(OC6H4OMe-o)2)]

There total 1 articles about (AuCl)2[(μ-PhN(P(OC6H4OMe-o)2)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1145951-91-2
[(Au2Cl2)2(μ-phenylene-1,4-diaminotetra(phosphonite))]

: 7732-18-5
water

: 791070-36-5
PhN(P(OC₆H₄OMe-o)2)2

: 1013639-52-5
(C₆H₅N(P(OC₆H₄OCH₃)2)2)Au₂Cl₂

: Au₂Cl₂(NH₂C₆H₄N(P(OC₆H₄OCH₃)2)2)

Guidance literature:: In dichloromethane; under anaerobic conditions, protected from light by wrapping with Al foil; soln. of PhN(P(OC6H4OMe)2)2 reacted with soln. of Au complex in CH2Cl2 in presence of trace amt. of moisture; detd. by (14)P NMR spectra;
DOI:10.1021/ic900085e

Reference yield: 82.0%

: 1013639-52-5
(AuCl)2[(μ-PhN(P(OC6H4OMe-o)2)]

: 791070-36-5
PhN(P(OC₆H₄OMe-o)2)2

: 1013639-53-6
AuCl[PhN(P(OC₆H₄OMe-o)2)2]

Guidance literature:: In tetrahydrofuran; (under anaerobic conditions, Schlenk); soln. of ligand in THF added dropwise to soln. of Au-complex in THF, refluxed for 4 h, cooled to room temp.; concd., layered with hexane, kept at -30°C for 1 d; elem. anal.;
DOI:10.1021/ic702133f

Reference yield: 81.0%

: 366-18-7
[2,2]bipyridinyl

: 1013639-52-5
(AuCl)2[(μ-PhN(P(OC6H4OMe-o)2)]

: silver perchlorate

: [Au2(2,2'-bipyridine)2[μ-PhN(P(OC6H4OMe-o)2)2]

Guidance literature:: In dichloromethane; (under anaerobic conditions, Schlenk); soln. of Au-complex and AgClO4 inCH2Cl2 stirred at room temp. for 2 h, filtered, soln. of 2,2'-bipyridin e in CH2Cl2 added at room temp., stirred for 2 h; concd. under vac., layered with hexane, kept at -30°C; elem. anal.;
DOI:10.1021/ic702133f