{(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃}

Base Information

Chemical Name:{(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃}
CAS No.:143806-76-2
Molecular Formula:C₂₆H₃₄GeN₂O₂S
Molecular Weight:511.224
Hs Code.:

{(CH<sub>3</sub>)3C<sub>6</sub>H<sub>2</sub>}2Ge{N(CH<sub>3</sub>)2}NH{(C<sub>4</sub>H<sub>2</sub>S)COOCH<sub>3</sub>}

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Chemical Property of {(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃}

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Technology Process of {(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃}

There total 3 articles about {(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 135302-94-2
N-dimesitylchlorogermyl-3-amino-2-methyl thiophoate

: 866-37-5
triethylgermyl dimethylamine

: 143806-76-2
{(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃}

Guidance literature:: In chloroform-d1; byproducts: (C2H5)3GeCl; addn. of Et3GeNMe2 to a soln. of Mes2Ge(Cl)NHTP (CDCl3), then the mixture is heated (20°C, 45min); evaporation of the solvants (1E-2 mmHg);
DOI:10.1016/0022-328X(92)83281-L

Reference yield: 53.0%

: 135302-94-2
N-dimesitylchlorogermyl-3-amino-2-methyl thiophoate

: 3585-33-9
lithium dimethylamide

: 143806-76-2
{(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃}

Guidance literature:: In tetrahydrofuran; benzene; byproducts: LiCl; addn. of Me2NLi (THF) to a soln. of Mes2Ge(Cl)NHTP in benzene, the mixture is stirred at 20°C (3h), (under inert gas); evaporation under reduced pressure, dissolving in benzene, filtration;
DOI:10.1016/0022-328X(92)83281-L

Reference yield: 27.0%

: 143806-72-8
{(CH₃)3(C₆H₂)}2GeN{(C₄H₂S)COOCH₃}

: 124-40-3
dimethyl amine

: 143806-76-2
{(CH₃)3C₆H₂}2Ge{N(CH₃)2}NH{(C₄H₂S)COOCH₃}

Guidance literature:: In benzene; addn. of anhydre Me2NH (excess) to a soln. of Mes2GeNTP (C6H6) at 60°C (48h) in a NMR tube; detected by (1)H NMR;
DOI:10.1016/0022-328X(92)83281-L