*,R^*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone>

Base Information

• Chemical Name: *,R^*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone>
• CAS No.: 152290-04-5
• Molecular Formula: C₃₀H₂₈N₂O₆
• Molecular Weight: 512.562

Synonyms:

Chemical Property of *,R^*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone>

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of *,R^*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone>

There total 3 articles about *,R^*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone> which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-benzenediacetic acid (19806-17-8) → *,R*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone> (152290-04-5)

Guidance literature:

Multi-step reaction with 2 steps

1: oxalyl chloride, DMF / CH₂Cl₂ / 18 h / Ambient temperature

2: 1) n-BuLi / 1) THF, hexane, -78 deg C, 25 min, 2) THF, -78 deg C, 4 h

With n-butyllithium; oxalyl dichloride; N,N-dimethyl-formamide; In dichloromethane;

DOI:10.1016/S0040-4020(01)85733-1

Reference yield:

1,3-phenylenediacetic acid dichloride (52584-23-3) + (S)-4-Benzyl-2-oxazolidinone (90719-32-7) → *,R*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone> (152290-04-5)

Guidance literature:

With n-butyllithium; Yield given. Multistep reaction; 1) THF, hexane, -78 deg C, 25 min, 2) THF, -78 deg C, 4 h;

DOI:10.1016/S0040-4020(01)85733-1

Reference yield:

(S)-4-Benzyl-2-oxazolidinone (90719-32-7) + benzene-1,3-dicarbonyl dichloride (99-63-8) → *,R*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone> (152290-04-5)

Guidance literature:

With n-butyllithium; triphenylmethane; sodium hydrogencarbonate; Yield given. Multistep reaction; 1.) hexane, THF, -78 deg C, 2.) hexane, THF, -78 deg C, 3.) hexane, THF, 25 deg C, 30 min;

DOI:10.1016/S0040-4020(96)00344-4

upstream raw materials:

1,3-phenylenediacetic acid dichloride

(S)-4-Benzyl-2-oxazolidinone

benzene-1,3-dicarbonyl dichloride

1,3-benzenediacetic acid

Downstream raw materials:

(S)-Azido-[3-((S)-azido-carboxy-methyl)-phenyl]-acetic acid

(S,S,S,S)-α,α'-diazido-β,β'-bis(4-benzyl-2-oxo-3-oxazolidinyl)-β,β'-dioxo-1,3-diethylbenzene

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 152290-04-5 *,R^*)>-3,3'-<1,3-Phenylenebis(1-oxo-2,1-ethanediyl)>bis<4-(phenylmethyl)-2-oxazolidinone>

Send

Send

Metric Ton KG G Pound L ML

Send

Send