2,3-BIS(CHLOROMETHYL)PYRIDINE

Base Information

Chemical Name:2,3-BIS(CHLOROMETHYL)PYRIDINE
CAS No.:45754-12-9
Molecular Formula:C7H7 Cl2 N
Molecular Weight:176.045
Hs Code.:2933399090
Mol file:45754-12-9.mol

Synonyms:2,3-Bis(chloromethyl)pyridine;

Suppliers and Price of 2,3-BIS(CHLOROMETHYL)PYRIDINE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
2,3-bis(chloromethyl)-Pyridine 97.00%
5G
$ 3230.00

Anichem
2,3-bis(chloromethyl)pyridine >95%
5g
$ 450.00

Anichem
2,3-bis(chloromethyl)pyridine >95%
1g
$ 150.00

BroadPharm
2,3-bis(chloromethyl)pyridine
100 MG
$ 190.00

Labseeker
2,3-BIS(CHLOROMETHYL)PYRIDINE 95
50g
$ 2666.00

AccelPharmtech
2,3-bis(chloromethyl)-Pyridine 97.00%
1G
$ 1890.00

Total 35 raw suppliers

Chemical Property of 2,3-BIS(CHLOROMETHYL)PYRIDINE

Chemical Property:

Vapor Pressure:0.016mmHg at 25°C
Refractive Index:1.548
Boiling Point:264.48 ºC at 760 mmHg
PKA:2.94±0.22(Predicted)
Flash Point:139.294 ºC
PSA：12.89000
Density:1.275 g/cm³
LogP:2.55920

Purity/Quality:

99% ^*data from raw suppliers

2,3-bis(chloromethyl)-Pyridine 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2,3-BIS(CHLOROMETHYL)PYRIDINE

There total 8 articles about 2,3-BIS(CHLOROMETHYL)PYRIDINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 423169-40-8
2,3-bis(hydroxymethyl)pyridine hydrochloride

: 45754-12-9
2,3-bis(chloromethyl)-pyridine

Guidance literature:: With thionyl chloride; In toluene;
DOI:10.1021/op3002728

Reference yield: 40.0%

: 38070-79-0
2,3-bis(hydroxymethyl)pyridine

: 45754-12-9
2,3-bis(chloromethyl)-pyridine

Guidance literature:: With thionyl chloride; In dichloromethane; at 45 ℃; Cooling with ice;

Reference yield:

: 605-38-9
dimethyl 2,3-pyridinedicarboxylate

: 45754-12-9
2,3-bis(chloromethyl)-pyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / NaBH₄ / ethanol / 17 h / Heating

2: 26 percent / SOCl₂ / CH₂Cl₂ / 1 h / 75 °C

With sodium tetrahydroborate; thionyl chloride; In ethanol; dichloromethane;
DOI:10.1016/S0968-0896(02)00426-1