(2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal

Base Information

Chemical Name:(2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal
CAS No.:53098-55-8
Molecular Formula:C₁₉H₂₆BrN₃O₇
Molecular Weight:488.335
Hs Code.:

Synonyms:

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Chemical Property of (2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal

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Technology Process of (2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal

There total 6 articles about (2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 400-91-9
1-bromo-3-fluoro-4,6-dinitrobenzene

: 53098-55-8
(2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogen carbonate / methanol / 3 h

With sodium hydrogencarbonate; In methanol;
DOI:10.1139/v80-080

Reference yield:

: 51067-70-0,53152-54-8
(4E,6E)-8-Amino-3-methoxy-2,4-dimethyl-octa-4,6-dienal

: 53098-55-8
(2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogen carbonate / methanol / 3 h

With sodium hydrogencarbonate; In methanol;
DOI:10.1139/v80-080

Reference yield:

: aurodox

: 53098-55-8
(2R,3S,4E,6E)-8-<(3-bromo-4,6-dinitrophenyl)amino>-3-methoxy-2,4-dimethyl-4,6-octadienal dimethyl acetal

Guidance literature:: Multi-step reaction with 5 steps

1: dimethylformamide / 72 h / Ambient temperature

2: acetic acid / 72 h / Ambient temperature

3: sodium metaperiodate

4: sodium hydrogen carbonate / methanol / 3 h

With sodium periodate; sodium hydrogencarbonate; acetic acid; In methanol; N,N-dimethyl-formamide;
DOI:10.1139/v80-080