tris(α-phenyl ethyl)boroxine

Base Information

Chemical Name:tris(α-phenyl ethyl)boroxine
CAS No.:4776-49-2
Molecular Formula:C₂₄H₂₇B₃O₃
Molecular Weight:395.91
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tris(α-phenyl ethyl)boroxine

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Technology Process of tris(α-phenyl ethyl)boroxine

There total 2 articles about tris(α-phenyl ethyl)boroxine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 121-43-7,63156-11-6
Trimethyl borate

: 672-65-1
(1-chloroethyl)benzene

: 4776-49-2
tris(α-phenyl ethyl)boroxine

Guidance literature:: With hydrogenchloride; magnesium; In tetrahydrofuran; diethyl ether; byproducts: 2.3-diphenyl butane, H2O; preparation of Grignard-compound in THF at -5°C, addn. to B(OCH3)3 in ether at -25°C, acidic hydrolysis, filtartion of diphenyl butane, removal of further volatile components by distn. in vac. (180-190°C/0.1Torr);;
DOI:10.1039/j29670000017