4-ammino>fenilacetato d'etile

Base Information

Chemical Name:4-ammino>fenilacetato d'etile
CAS No.:77440-24-5
Molecular Formula:C₂₅H₃₃NO₄
Molecular Weight:411.541
Hs Code.:

4-<N-<3-(2-cicloesilfenossi)-2-idrossipropil>ammino>fenilacetato d'etile

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Suppliers and Price of 4-ammino>fenilacetato d'etile

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-ammino>fenilacetato d'etile

Chemical Property:

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Technology Process of 4-ammino>fenilacetato d'etile

There total 1 articles about 4-ammino>fenilacetato d'etile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 67006-90-0
(2,3-epossipropossi)-2-cicloesilbenzene

: 5438-70-0
ethyl (4-amino-3,5-dibromophenyl)acetate

: 77440-24-5
4-ammino>fenilacetato d'etile

Guidance literature:: In ethanol; for 16h; Heating;

Reference yield:

: 77440-24-5
4-ammino>fenilacetato d'etile

: {4-[2-(2-Cyclohexyl-phenoxymethyl)-morpholin-4-yl]-phenyl}-acetic acid; hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1: 1.) NaOH / 1.) CH₂Cl₂, water, 0 deg C, 2.) CH₂Cl₂, water, 0 deg C, 2 h.

2: 69 percent / 1N NaOH / ethanol / 24 h / Heating

3: 57 percent / DCCI, pyridine / tetrahydrofuran / 48 h / Ambient temperature

4: 1.) B₂H₆, 2.) 5 N HCl / 1.) THF, 1h. room temp., then 4 h. reflux, 2.) 0 deg C

5: 1.) 1.045 N NaOH, 2.) gaseous HCl / 1.) aq. ethanol, 3 h., reflux

With pyridine; hydrogenchloride; sodium hydroxide; dicyclohexyl-carbodiimide; diborane; In tetrahydrofuran; ethanol;

Reference yield:

: 77440-24-5
4-ammino>fenilacetato d'etile

: {4-[2-(2-Cyclohexyl-phenoxymethyl)-morpholin-4-yl]-phenyl}-acetic acid pentachlorophenyl ester; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaOH / 1.) CH₂Cl₂, water, 0 deg C, 2.) CH₂Cl₂, water, 0 deg C, 2 h.

2: 69 percent / 1N NaOH / ethanol / 24 h / Heating

3: 57 percent / DCCI, pyridine / tetrahydrofuran / 48 h / Ambient temperature

4: 1.) B₂H₆, 2.) 5 N HCl / 1.) THF, 1h. room temp., then 4 h. reflux, 2.) 0 deg C

With pyridine; hydrogenchloride; sodium hydroxide; dicyclohexyl-carbodiimide; diborane; In tetrahydrofuran; ethanol;