6-AMINO-5-BROMONICOTINIC ACID

Base Information

• Chemical Name: 6-AMINO-5-BROMONICOTINIC ACID
• CAS No.: 180340-69-6
• Molecular Formula: C6H5BrN2O2
• Molecular Weight: 217.022
• Hs Code.: 2933399090
• Mol file: 180340-69-6.mol

Synonyms:6-Amino-5-bromonicotinicacid;6-Amino-5-bromopyridine-3-carboxylic acid;6-Amino-5-bromonicotinic acid;

Chemical Property of 6-AMINO-5-BROMONICOTINIC ACID

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.685
• Boiling Point: 378.001 °C at 760 mmHg
• PKA: 3.94±0.20(Predicted)
• Flash Point: 182.409 °C
• PSA: 76.21000
• Density: 1.91 g/cm³
• LogP: 1.70570

Purity/Quality:

99%, ^*data from raw suppliers

6-Amino-5-bromonicotinicAcid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6-AMINO-5-BROMONICOTINIC ACID

There total 4 articles about 6-AMINO-5-BROMONICOTINIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

methyl 6-amino-5-bromopyridine-3-carboxylate (180340-70-9) → 6-Amino-5-bromopyridine-3-carboxylic acid (180340-69-6)

Guidance literature:

With potassium hydroxide; In methanol; for 5h; Reflux;

Reference yield:

6-aminonicotinic acid (3167-49-5) → 6-Amino-5-bromopyridine-3-carboxylic acid (180340-69-6)

Guidance literature:

With bromine; In water; acetic acid;

Reference yield:

6-amino-5-bromonicotinic acid ethyl ester (850429-51-5) → 6-Amino-5-bromopyridine-3-carboxylic acid (180340-69-6)

Guidance literature:

6-amino-5-bromonicotinic acid ethyl ester; With water; potassium hydroxide; In methanol; at 60 ℃; for 3h;

With hydrogenchloride; In methanol; water;

upstream raw materials:

6-aminonicotinic acid

6-amino-5-bromonicotinic acid ethyl ester

methyl 6-amino-5-bromopyridine-3-carboxylate

Downstream raw materials:

methyl 6-amino-5-bromopyridine-3-carboxylate

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