(C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2

Base Information

Chemical Name:(C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2
CAS No.:944133-13-5
Molecular Formula:C₆₂H₆₂N₆NiO₂
Molecular Weight:981.903
Hs Code.:

(C(CH<sub>3</sub>)3C<sub>6</sub>H<sub>4</sub>)4C<sub>20</sub>H<sub>6</sub>N<sub>4</sub>Ni(NHCOH)2

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Chemical Property of (C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2

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Technology Process of (C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2

There total 2 articles about (C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 64-18-6
formic acid

: (C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NH₂)2

: 944133-13-5
(C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2

: C₆₁H₆₀N₆Ni*H₂O

Guidance literature:: formic acid; (C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NH₂)2; In toluene; for 2h; Reflux; Inert atmosphere;

With potassium carbonate; In toluene;
DOI:10.1002/ejoc.200901310

Reference yield:

: 16940-66-2
sodium tetrahydroborate

: 64-18-6
formic acid

: 944133-11-3
(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNO₂NH₂

: 944133-08-8
(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiCHN₂H

: 944133-12-4
(C(CH₃)3C₆H₄)4C₂₀H₆N₄NiNH₂NHCOH

: 944133-13-5
(C(CH₃)3C₆H₄)4C₂₀H₆N₄Ni(NHCOH)2

Guidance literature:: With Pd/C; In methanol; dichloromethane; toluene; Ni complex reacted with NaBH4 in CH2Cl2/CH3OH in the presence of Pd/C at25°C for 1 h, treated with formic acid in toluene (1:1), refluxe d for 10 min at 110°C; chromy.(silica gel);
DOI:10.1039/b704681b