2,3-Difluoro-4'-propyl-1,1'-Biphenyl

Base Information

Chemical Name:2,3-Difluoro-4'-propyl-1,1'-Biphenyl
CAS No.:126163-02-8
Molecular Formula:C15H14F2
Molecular Weight:232.273
Hs Code.:
DSSTox Substance ID:DTXSID70568809
Wikidata:Q72464136
Mol file:126163-02-8.mol

Synonyms:126163-02-8;2,3-Difluoro-4'-propyl-1,1'-Biphenyl;2,3-DIFLUORO-4'-PROPYLBIPHENYL;1,2-difluoro-3-(4-propylphenyl)benzene;1,1'-Biphenyl, 2,3-difluoro-4'-propyl-;2,3-Difluoro-4/'-propyl-1,1/'-biphenyl;SCHEMBL1599469;AMY8664;DTXSID70568809;AKOS015917654;SB66758;AC-23888

Suppliers and Price of 2,3-Difluoro-4'-propyl-1,1'-Biphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
2,3-Difluoro-4'-propyl-1,1'-biphenyl 95+%
1g
$ 772.00

Arctom
2,3-Difluoro-4'-propyl-1,1'-biphenyl ≥95%
1g
$ 622.00

American Custom Chemicals Corporation
2,3-DIFLUORO-4'-PROPYL-1,1'-BIPHENYL 95.00%
5MG
$ 505.59

Total 32 raw suppliers

Chemical Property of 2,3-Difluoro-4'-propyl-1,1'-Biphenyl

Chemical Property:

Boiling Point:302.1 °C at 760 mmHg
Flash Point:113.8 °C
PSA：0.00000
Density:1.093 g/cm³
LogP:4.58430
Storage Temp.:2-8°C
XLogP3:5.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:232.10635677
Heavy Atom Count:17
Complexity:221

Purity/Quality:

98%,99%, ^*data from raw suppliers

2,3-Difluoro-4'-propyl-1,1'-biphenyl 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC1=CC=C(C=C1)C2=C(C(=CC=C2)F)F

Technology Process of 2,3-Difluoro-4'-propyl-1,1'-Biphenyl

There total 4 articles about 2,3-Difluoro-4'-propyl-1,1'-Biphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 588-93-2
p-bromo-n-propylbenzene

: 121219-16-7
(2,3-difluorophenyl)boronic acid

: 126163-02-8
2,3-difluoro-4-(4-propylphenyl)benzene

Guidance literature:: p-bromo-n-propylbenzene; (2,3-difluorophenyl)boronic acid; With potassium carbonate; In water; acetone; for 0.333333h; Inert atmosphere; Reflux;

With palladium diacetate; In water; acetone; for 6h; Inert atmosphere; Reflux;
DOI:10.1039/c3tc31461h

Reference yield:

: 367-11-3
ortho-difluorobenzene

: 126163-02-8
2,3-difluoro-4-(4-propylphenyl)benzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium / tetrahydrofuran

1.3: Acidic conditions

2.1: potassium carbonate / water; acetone / 0.33 h / Inert atmosphere; Reflux

2.2: 6 h / Inert atmosphere; Reflux

With n-butyllithium; potassium carbonate; In tetrahydrofuran; water; acetone; 2.1: |Suzuki-Miyaura Coupling / 2.2: |Suzuki-Miyaura Coupling;
DOI:10.1039/c3tc31461h