methyl 3-methyl-4-phenyl-4--butanoate

Base Information

Chemical Name:methyl 3-methyl-4-phenyl-4--butanoate
CAS No.:101073-98-7
Molecular Formula:C₁₉H₂₂N₂O₄S
Molecular Weight:374.461
Hs Code.:

methyl 3-methyl-4-phenyl-4-<N'-(p-toluenesulfonyl)hydrazono>-butanoate

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-methyl-4-phenyl-4--butanoate

Chemical Property:

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Technology Process of methyl 3-methyl-4-phenyl-4--butanoate

There total 5 articles about methyl 3-methyl-4-phenyl-4--butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 72315-95-8
methyl 3-methyl-4-oxo-4-phenylbutanoate

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 101073-98-7
methyl 3-methyl-4-phenyl-4--butanoate

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 4h; Heating;

Reference yield:

: 2166-31-6
6-phenylpyridazin-3(2H)-one

: 101073-98-7
methyl 3-methyl-4-phenyl-4--butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 70 percent / NaH / tetrahydrofuran / 1.5 h / Ambient temperature

2: 0 deg C, 14 h, then quenched with R-OH

With sodium hydride; In tetrahydrofuran;

Reference yield:

: 51765-79-8
3-methyl-4-oxo-4-phenylbutanenitrile

: 101073-98-7
methyl 3-methyl-4-phenyl-4--butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / conc. H₂SO₄ / 8 h / Heating

2: 55 percent / p-TsOH / benzene / 4 h / Heating

With sulfuric acid; toluene-4-sulfonic acid; In benzene;