(CH₃)3SnC(C₆H₅)CHCHO

Base Information

Chemical Name:(CH₃)3SnC(C₆H₅)CHCHO
CAS No.:180070-93-3
Molecular Formula:C₁₂H₁₆OSn
Molecular Weight:294.968
Hs Code.:

(CH<sub>3</sub>)3SnC(C<sub>6</sub>H<sub>5</sub>)CHCHO

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (CH₃)3SnC(C₆H₅)CHCHO

Chemical Property:

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Technology Process of (CH₃)3SnC(C₆H₅)CHCHO

There total 1 articles about (CH₃)3SnC(C₆H₅)CHCHO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 4885-02-3
Dichloromethyl methyl ether

: 27471-13-2,85271-56-3
(Z)-(1-phenylethene-1,2-diyl)bis(trimethylstannane)

: 180070-93-3,180070-94-4
(CH₃)3SnC(C₆H₅)CHCHO

Guidance literature:: With aluminium trichloride; In dichloromethane; byproducts: Me3SnCl; Ar-atmosphere; slow addn. of Sn-compd. and Cl2CHOMe to AlCl3 at -78°C, stirring (-78°C, 4 h); addn. od satd. aq. NH4Cl, extn. of aq. layer (CH2Cl2), stirring of org. layer with aq. KF for 3 h, filtration off of Me3SnF, extn. into CH2Cl2, drying, evapn. off of solvent, distn.; isomer mixt. not sepd., detd. by NMR, IR and mass spectroscopy;
DOI:10.1016/S0022-328X(96)06151-7

Reference yield:

: 180070-93-3,180070-94-4
(CH₃)3SnC(C₆H₅)CHCHO

: 74-94-2
dimethylamine borane

: 180070-98-8
Z-3-phenyl-3-trimethylstannyl-prop-2-ene-1-ol

: 180070-97-7
E-3-phenyl-3-trimethylstannyl-prop-2-ene-1-ol

Guidance literature:: In diethyl ether; Ar-atmosphere; stirring at room temp. for 5 h; water addn., extn. of aq. layer (Et2O), drying (MgSO4), distn. off of solvent; isomer mixt. not sepd., detd. by NMR spectroscopy;
DOI:10.1016/S0022-328X(96)06151-7