C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Base Information

Chemical Name:C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾
CAS No.:1423692-01-6
Molecular Formula:C₂₈H₂₃N₂O₄S*Na
Molecular Weight:506.557
Hs Code.:

C<sub>28</sub>H<sub>23</sub>N<sub>2</sub>O<sub>4</sub>S<sup>(1-)</sup>*Na<sup>(1+)</sup>

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Chemical Property of C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

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Technology Process of C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

There total 11 articles about C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 124276-67-1
1-(4-bromophenyl)cyclopropanecarbonitrile

: 1423692-01-6
C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium hydroxide / ethylene glycol / 6 h / 160 °C

1.2: pH 3 - 4

2.1: sulfuric acid / 4 h / 65 °C

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

5.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

5.2: 0 °C / pH 4

6.1: sodium hydroxide / water; acetonitrile / 0.5 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; sodium carbonate; potassium hydroxide; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; ethylene glycol; acetonitrile;

Reference yield:

: 345965-52-8
1-(4-bromophenyl)cyclopropanecarboxylic acid

: 1423692-01-6
C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 4 h / 65 °C

2.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere

3.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

4.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

4.2: 0 °C / pH 4

5.1: sodium hydroxide / water; acetonitrile / 0.5 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; sodium carbonate; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; acetonitrile;

Reference yield:

: 16532-79-9
4-Bromophenylacetonitrile

: 1423692-01-6
C₂₈H₂₃N₂O₄S^(1-)*Na⁽¹⁺⁾

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetrabutylammomium bromide; potassium hydroxide / water; toluene / 65 °C

2.1: potassium hydroxide / ethylene glycol / 6 h / 160 °C

2.2: pH 3 - 4

3.1: sulfuric acid / 4 h / 65 °C

4.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 90 °C / Inert atmosphere

5.1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium carbonate / water; 1,2-dimethoxyethane / 80 °C / Inert atmosphere

6.1: sodium t-butanolate / tetrahydrofuran; acetonitrile / 20 °C

6.2: 0 °C / pH 4

7.1: sodium hydroxide / water; acetonitrile / 0.5 h / 0 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sulfuric acid; tetrabutylammomium bromide; sodium carbonate; potassium hydroxide; sodium hydroxide; sodium t-butanolate; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water; ethylene glycol; toluene; acetonitrile;