Technology Process of 6-methoxy-2,3,4-trimethylphenylboronic acid
There total 1 articles about 6-methoxy-2,3,4-trimethylphenylboronic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
butyllithium;
In
tetrahydrofuran;
BuLi addn. to stirred org. compd. soln. at -78°C (N2), suspn. warming until solid dissolved, recooling to -78°C, stirring 1 h, B-compd. addn., stirring (-78°C/1.5 h, N2), warming to room temp., water addn., Et2O addn.; org. layer washing (satd. as. Na2SO4), drying (Na2SO4), filtration, solvent evapn. at 35°C, residue pulverization, air drying 2 d, stiring with pentane for 2 h, washings discarding; elem. anal.;
DOI:10.1039/p19960002173
- Guidance literature:
-
In
chloroform;
B-compd. addn. to Pb-compd. soln., mixt. stirring at room temp. for 2 d,suspn. washing (water), chloroform soln. drying (Na2SO4), solvent evapn .; crystn. (CH2Cl2/light petroleum); elem. anal.;
DOI:10.1039/p19960002173
