benzaldehyde 2-naphthyloxyacetamidoacetohydrazone

Base Information

Chemical Name:benzaldehyde 2-naphthyloxyacetamidoacetohydrazone
CAS No.:1285706-00-4
Molecular Formula:C₂₁H₁₉N₃O₃
Molecular Weight:361.4
Hs Code.:

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Chemical Property of benzaldehyde 2-naphthyloxyacetamidoacetohydrazone

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Technology Process of benzaldehyde 2-naphthyloxyacetamidoacetohydrazone

There total 6 articles about benzaldehyde 2-naphthyloxyacetamidoacetohydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.8%

: 443293-74-1
2-naphthyloxyacetamidoacetohydrazide

: 100-52-7
benzaldehyde

: 1285706-00-4
benzaldehyde 2-naphthyloxyacetamidoacetohydrazone

Guidance literature:: In methanol; at 20 ℃;
DOI:10.1111/j.1747-0285.2010.01050.x

Reference yield:

: 6036-14-2
ethyl (naphthalen-2-yloxy)acetate

: 1285706-00-4
benzaldehyde 2-naphthyloxyacetamidoacetohydrazone

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrazine hydrate / ethanol / 6 h / Reflux

2.1: hydrogenchloride; acetic acid; sodium nitrite / water / 0.25 h / Cooling with ice

3.1: triethylamine / ethyl acetate / 0.5 h / 0 °C

3.2: 24 h / -5 - 20 °C

4.1: hydrazine hydrate / ethanol / 6 h / Reflux

5.1: methanol / 20 °C

With hydrogenchloride; hydrazine hydrate; acetic acid; triethylamine; sodium nitrite; In methanol; ethanol; water; ethyl acetate;
DOI:10.1111/j.1747-0285.2010.01050.x

Reference yield:

: 36304-47-9
1-(2-naphthyloxyacetyl)hydrazine

: 1285706-00-4
benzaldehyde 2-naphthyloxyacetamidoacetohydrazone

Guidance literature:: Multi-step reaction with 4 steps

1.1: hydrogenchloride; acetic acid; sodium nitrite / water / 0.25 h / Cooling with ice

2.1: triethylamine / ethyl acetate / 0.5 h / 0 °C

2.2: 24 h / -5 - 20 °C

3.1: hydrazine hydrate / ethanol / 6 h / Reflux

4.1: methanol / 20 °C

With hydrogenchloride; hydrazine hydrate; acetic acid; triethylamine; sodium nitrite; In methanol; ethanol; water; ethyl acetate;
DOI:10.1111/j.1747-0285.2010.01050.x