Technology Process of (1R,2R)-2-Benzenesulfonylmethyl-cyclopropanecarbonitrile
There total 5 articles about (1R,2R)-2-Benzenesulfonylmethyl-cyclopropanecarbonitrile which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
dihydrogen peroxide;
ammonium molibdate;
In
methanol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 40 percent / n-butyl-lithium / tetrahydrofuran / 1 h / -30 °C
2: 57 percent / thionyl chloride, pyridine / CH2Cl2 / 2 h / Heating
3: 99 percent / methanol / 16 h / Heating
4: 99 percent / H2O2 / ammonium molibdate / methanol
With
pyridine; n-butyllithium; thionyl chloride; dihydrogen peroxide;
ammonium molibdate;
In
tetrahydrofuran; methanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 74 percent / m-chloroperbenzoic acid / CHCl3 / 16 h / 20 °C
2: 40 percent / n-butyl-lithium / tetrahydrofuran / 1 h / -30 °C
3: 57 percent / thionyl chloride, pyridine / CH2Cl2 / 2 h / Heating
4: 99 percent / methanol / 16 h / Heating
5: 99 percent / H2O2 / ammonium molibdate / methanol
With
pyridine; n-butyllithium; thionyl chloride; dihydrogen peroxide; 3-chloro-benzenecarboperoxoic acid;
ammonium molibdate;
In
tetrahydrofuran; methanol; dichloromethane; chloroform;