Technology Process of 2,4-Pentadienenitrile
There total 9 articles about 2,4-Pentadienenitrile which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium ethanolate;
In
ethanol;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 40 percent / n-butyl-lithium / tetrahydrofuran / 1 h / -30 °C
2: 57 percent / thionyl chloride, pyridine / CH2Cl2 / 2 h / Heating
3: 99 percent / methanol / 16 h / Heating
4: 99 percent / H2O2 / ammonium molibdate / methanol
5: 1 M sodium ethoxide / ethanol / 20 °C
With
pyridine; n-butyllithium; thionyl chloride; dihydrogen peroxide; sodium ethanolate;
ammonium molibdate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 74 percent / m-chloroperbenzoic acid / CHCl3 / 16 h / 20 °C
2: 40 percent / n-butyl-lithium / tetrahydrofuran / 1 h / -30 °C
3: 57 percent / thionyl chloride, pyridine / CH2Cl2 / 2 h / Heating
4: 99 percent / methanol / 16 h / Heating
5: 99 percent / H2O2 / ammonium molibdate / methanol
6: 1 M sodium ethoxide / ethanol / 20 °C
With
pyridine; n-butyllithium; thionyl chloride; dihydrogen peroxide; sodium ethanolate; 3-chloro-benzenecarboperoxoic acid;
ammonium molibdate;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; chloroform;
