C₂₅H₂₉NO₄

Base Information

Chemical Name:C₂₅H₂₉NO₄
CAS No.:1401354-95-7
Molecular Formula:C₂₅H₂₉NO₄
Molecular Weight:407.51
Hs Code.:

C<sub>25</sub>H<sub>29</sub>NO<sub>4</sub>

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₂₉NO₄

Chemical Property:

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Technology Process of C₂₅H₂₉NO₄

There total 7 articles about C₂₅H₂₉NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1401354-82-2
α-tert-butoxycarbonyl-α-(2-methoxyphenyl)-γ-methylidene-δ-valerolactone

: 3173-56-6
benzyl isothiocyanate

: C₂₅H₂₉NO₄

: 1401354-95-7
C₂₅H₂₉NO₄

Guidance literature:: With allyl(cyclopentadiene)palladium(II); C₄₀H₃₆NO₂P; In toluene; at 30 ℃; for 12h; Overall yield = 53%;
DOI:10.1039/c2cc35259a

Reference yield:

: 93-25-4
2-methoxyphenylacetic acid

: C₂₅H₂₉NO₄

: 1401354-95-7
C₂₅H₂₉NO₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: thionyl chloride / 6 h / 0 - 20 °C

2.1: sodium hydride / mineral oil / 12 h / 0 - 20 °C

3.1: potassium hydroxide / methanol / 1.5 h / 20 °C

4.1: dmap; dicyclohexyl-carbodiimide / 1 h / 0 - 20 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 0.67 h / 0 °C

5.2: 48 h / 55 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 11 h / -65 - -5 °C

7.1: allyl(cyclopentadiene)palladium(II); C₄₀H₃₆NO₂P / toluene / 12 h / 30 °C

With dmap; thionyl chloride; allyl(cyclopentadiene)palladium(II); C₄₀H₃₆NO₂P; tetrabutyl ammonium fluoride; sodium hydride; dicyclohexyl-carbodiimide; potassium hydroxide; In tetrahydrofuran; methanol; toluene; mineral oil;
DOI:10.1039/c2cc35259a

Reference yield:

: 27798-60-3
methyl 2-(2-methoxyphenyl)acetate

: C₂₅H₂₉NO₄

: 1401354-95-7
C₂₅H₂₉NO₄

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium hydride / mineral oil / 12 h / 0 - 20 °C

2.1: potassium hydroxide / methanol / 1.5 h / 20 °C

3.1: dmap; dicyclohexyl-carbodiimide / 1 h / 0 - 20 °C

4.1: sodium hydride / tetrahydrofuran; mineral oil / 0.67 h / 0 °C

4.2: 48 h / 55 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 11 h / -65 - -5 °C

6.1: allyl(cyclopentadiene)palladium(II); C₄₀H₃₆NO₂P / toluene / 12 h / 30 °C

With dmap; allyl(cyclopentadiene)palladium(II); C₄₀H₃₆NO₂P; tetrabutyl ammonium fluoride; sodium hydride; dicyclohexyl-carbodiimide; potassium hydroxide; In tetrahydrofuran; methanol; toluene; mineral oil;
DOI:10.1039/c2cc35259a