Technology Process of C56H70N10O9
There total 12 articles about C56H70N10O9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C
2: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 16 h / 20 °C
With
triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/cmdc.201100241
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 0 - 20 °C
2.1: hydrazine hydrate / methanol / 16 h / 20 °C
2.2: 3 h / 20 °C
3.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 16 h / 20 °C
With
benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride;
In
methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201100241
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: hydrogenchloride / ethyl acetate / 2 h / 20 °C
2.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / acetonitrile / 16 h / 0 - 20 °C
3.1: hydrazine hydrate / methanol / 16 h / 20 °C
3.2: 3 h / 20 °C
4.1: triethylamine; mercury dichloride / N,N-dimethyl-formamide / 16 h / 20 °C
With
hydrogenchloride; benzotriazol-1-ol; hydrazine hydrate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; mercury dichloride;
In
methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1002/cmdc.201100241