Carbamic acid, N-[2-(4-pyridinyl)ethyl]-, 1,1-dimethylethylester

Base Information

Chemical Name:Carbamic acid, N-[2-(4-pyridinyl)ethyl]-, 1,1-dimethylethylester
CAS No.:109573-05-9
Molecular Formula:C12H18 N2 O2
Molecular Weight:222.287
Hs Code.:

Synonyms:Carbamic acid, [2-(4-pyridinyl)ethyl]-, 1,1-dimethylethylester (9CI);4-[2-(N-(tert-Butoxycarbonyl)amino)ethyl]pyridine;tert-butyl 2-(pyridin-4-yl)ethylcarbamate;

Suppliers and Price of Carbamic acid, N-[2-(4-pyridinyl)ethyl]-, 1,1-dimethylethylester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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Total 6 raw suppliers

Chemical Property of Carbamic acid, N-[2-(4-pyridinyl)ethyl]-, 1,1-dimethylethylester

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, N-[2-(4-pyridinyl)ethyl]-, 1,1-dimethylethylester

There total 1 articles about Carbamic acid, N-[2-(4-pyridinyl)ethyl]-, 1,1-dimethylethylester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-43-6,329041-72-7
4-vinylpyridine

: 109573-05-9
(tert-Butoxy)-N-<2-(4-pyridyl)ethyl>carbamat

Guidance literature:: Multi-step reaction with 2 steps

1: 46.9 g / ammonium chloride / H₂O; methanol / Heating

2: 2-methyl-propan-2-ol / 12 h / 20 °C

With ammonium chloride; In methanol; water; tert-butyl alcohol;
DOI:10.1021/jm051272l

Reference yield: 77.0%

: 109573-05-9
(tert-Butoxy)-N-<2-(4-pyridyl)ethyl>carbamat

: 17508-17-7
O-(2,4-dinitrophenyl)hydroxylamine

: N-amino-(4-[2-N-(tert-butyloxycarbonyl)aminoethyl]pyridinium)-2,4-dinitrophenolate

Guidance literature:: In dichloromethane; acetonitrile; at 20 ℃;
DOI:10.1002/open.201402031

Reference yield:

: 109573-05-9
(tert-Butoxy)-N-<2-(4-pyridyl)ethyl>carbamat

: C₃₄H₅₁N₅O₅S

Guidance literature:: Multi-step reaction with 3 steps

1: 21.9 g / H₂; AcOH / PtO₂ / 96 h / 35 °C

2: PyBop; diisopropylethylamine / dimethylformamide / 0 - 20 °C

3: aq. HCl; AcOH / 1 h / 20 °C

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In N,N-dimethyl-formamide;
DOI:10.1021/jm051272l