HMo(CO)2(PCy₃)(Cp)

Base Information

Chemical Name:HMo(CO)2(PCy₃)(Cp)
CAS No.:220206-24-6
Molecular Formula:C₂₅H₃₉MoO₂P
Molecular Weight:498.497
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of HMo(CO)2(PCy₃)(Cp)

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Technology Process of HMo(CO)2(PCy₃)(Cp)

There total 1 articles about HMo(CO)2(PCy₃)(Cp) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 12176-06-6
hydrido(tricarbonyl)(cyclopentadienyl)molybdenum

: 2622-14-2
tricyclohexylphosphine

: 220206-24-6,171776-15-1,298214-43-4
HMo(CO)2(PCy₃)(Cp)

Guidance literature:: In toluene; (Ar), heating (100°C, 8 h); washing (hexane); elem. anal.;
DOI:10.1021/ja9820036

Reference yield: 85.0%

: 220206-24-6,171776-15-1,298214-43-4
HMo(CO)2(PCy₃)(Cp)

: 341-02-6
trityl tetrafluoroborate

: 220206-23-5,298214-45-6,219968-59-9
(C₅H₅)(CO)2(P(C₆H₁₁)3)MoFBF₃

Guidance literature:: In dichloromethane; (Ar), stirring (-40°C, 40 min.); adding hexane, standing (-78°C, 3 h); elem. anal.;
DOI:10.1021/ja9820036

Reference yield: 84.0%

: 75-09-2
dichloromethane

: 220206-24-6,171776-15-1,298214-43-4
HMo(CO)2(PCy₃)(Cp)

: triphenylmethylium tetrakis[3,5-bis(trifluoromethyl)phenyl]borate

: Cp(CO)2(PCy₃)Mo(ClCH₂Cl)

Guidance literature:: In dichloromethane; under Ar using Schlenk or vac.-line technique; soln. of complex (0.602 mol) in CH2Cl2 added to cold (-30°C) soln. of (Ph3C)B(C6H3(CF3)2)4(0.573 mol) in CH2Cl2; stirred at -30°C for 20 min; vol. of solvent reduced; hexane added; ppt. filtered off; washed (hexane); dried (vac.); elem. anal.;
DOI:10.1016/j.ica.2009.02.028