C₂₂H₁₉N₃O

Base Information

• Chemical Name: C₂₂H₁₉N₃O
• CAS No.: 1351520-09-6
• Molecular Formula: C₂₂H₁₉N₃O
• Molecular Weight: 341.412
• Mol file: 1351520-09-6.mol

Synonyms:

Chemical Property of C₂₂H₁₉N₃O

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₂H₁₉N₃O

There total 6 articles about C₂₂H₁₉N₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H21N3O (1351520-08-5) → C22H19N3O (1351520-09-6)

Guidance literature:

With selenium(IV) oxide; In 1,4-dioxane; at 110 ℃; for 24h;

DOI:10.1002/adsc.201100210

Reference yield:

2.6-bis(hydroxymethyl)pyridine (1195-59-1) → C22H19N3O (1351520-09-6)

Guidance literature:

Multi-step reaction with 3 steps

1: selenium(IV) oxide / 1,4-dioxane / 48 h / 65 °C / Inert atmosphere; Ultrasonic bath

2: sodium dithionite / ethyl methyl ether; water / 24 h / 100 °C

3: selenium(IV) oxide / 1,4-dioxane / 24 h / 110 °C

With selenium(IV) oxide; sodium dithionite; In 1,4-dioxane; ethyl methyl ether; water;

DOI:10.1002/adsc.201100210

Reference yield:

ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → C22H19N3O (1351520-09-6)

Guidance literature:

Multi-step reaction with 3 steps

1: potassium fluoride / 48 h / 180 °C / Inert atmosphere

2: sodium dithionite / ethyl methyl ether; water / 24 h / 100 °C

3: selenium(IV) oxide / 1,4-dioxane / 24 h / 110 °C

With selenium(IV) oxide; potassium fluoride; sodium dithionite; In 1,4-dioxane; ethyl methyl ether; water;

DOI:10.1002/adsc.201100210

upstream raw materials:

6-(hydroxymethyl)picolinaldehyde

2.6-bis(hydroxymethyl)pyridine

C₂₂H₂₁N₃O

2-(2’,4’,6’-trimethylanilido)nitrobenzene

Downstream raw materials:

C₂₂H₁₉N₃O₂

Refernces