N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide

Base Information

Chemical Name:N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide
CAS No.:288249-52-5
Molecular Formula:C₂₃H₂₄N₄O₂
Molecular Weight:388.469
Hs Code.:

Synonyms:

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Chemical Property of N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide

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Technology Process of N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide

There total 8 articles about N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 10199-53-8
1-Methyl-5-phenyl-1H-pyrazole-3-carboxylic acid

: 206885-36-1
5-amino-2-neopentyloxybenzonitrile

: 288249-52-5
N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide

Guidance literature:: With diethylphosphoryl cyanide; triethylamine; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 1h;

Reference yield:

: 2516-96-3
2-chloro-5-nitrobenzoic acid

: 288249-52-5
N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide

Guidance literature:: Multi-step reaction with 5 steps

1.1: thionyl chloride / DMF (N,N-dimethyl-formamide); toluene / 3 h / 20 °C / Heating / reflux

1.2: Ice cooling

2.1: benzenesulfonyl chloride / DMF (N,N-dimethyl-formamide); toluene / 3 h / 20 - 145 °C

3.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h / Ice cooling

4.1: iron; ammonium chloride / ethanol; water / 0.83 h / 65 °C / Heating / reflux

5.1: diethylphosphoryl cyanide; triethylamine / DMF (N,N-dimethyl-formamide) / 1 h / 20 °C

With thionyl chloride; diethylphosphoryl cyanide; iron; sodium hydride; ammonium chloride; triethylamine; benzenesulfonyl chloride; In DMF (N,N-dimethyl-formamide); ethanol; water; toluene;

Reference yield:

: 10250-65-4
methyl 1-methyl-5-phenyl-1H-pyrazole-3-carboxylate

: 288249-52-5
N-(3-cyano-4-neopentyloxyphenyl)-1-methyl-5-phenylpyrazole-3-carboxyamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / ethanol; water / 0.5 h / Heating / reflux

2: diethylphosphoryl cyanide; triethylamine / DMF (N,N-dimethyl-formamide) / 1 h / 20 °C

With sodium hydroxide; diethylphosphoryl cyanide; triethylamine; In DMF (N,N-dimethyl-formamide); ethanol; water;