C₃₇H₂₄N₂

Base Information

Chemical Name:C₃₇H₂₄N₂
CAS No.:1315500-79-8
Molecular Formula:C₃₇H₂₄N₂
Molecular Weight:496.611
Hs Code.:

C<sub>37</sub>H<sub>24</sub>N<sub>2</sub>

Synonyms:

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Chemical Property of C₃₇H₂₄N₂

Chemical Property:

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Technology Process of C₃₇H₂₄N₂

There total 10 articles about C₃₇H₂₄N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 577-19-5
2-nitrophenyl bromide

: 1315500-79-8
C₃₇H₂₄N₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium acetate / 8 h / 180 °C / Inert atmosphere

2.1: sodium dithionite / ethyl acetate; water; tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

2.2: 1 h / 20 °C

3.1: toluene-4-sulfonic acid / xylene / 3 h / Reflux

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 8 h / Inert atmosphere; Reflux

With sodium dithionite; sodium acetate; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; toluene-4-sulfonic acid; In tetrahydrofuran; 1,2-dimethoxyethane; water; ethyl acetate; xylene;

Reference yield:

: 40138-16-7
2-formylbenzene boronic acid

: 1315500-79-8
C₃₇H₂₄N₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 8 h / Inert atmosphere; Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3.1: methanesulfonic acid / dichloromethane / 8 h / 20 °C

4.1: n-butyllithium / hexane; diethyl ether / 1 h / -40 - 0 °C / Inert atmosphere

4.2: 5 h / -60 - 20 °C

5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 8 h / Inert atmosphere; Reflux

With n-butyllithium; methanesulfonic acid; potassium tert-butylate; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane; water;

Reference yield:

: 83-53-4
1,4-dibromonaphthalene

: 1315500-79-8
C₃₇H₂₄N₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 8 h / Inert atmosphere; Reflux

2.1: potassium tert-butylate / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

3.1: methanesulfonic acid / dichloromethane / 8 h / 20 °C

4.1: n-butyllithium / hexane; diethyl ether / 1 h / -40 - 0 °C / Inert atmosphere

4.2: 5 h / -60 - 20 °C

5.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 8 h / Inert atmosphere; Reflux

With n-butyllithium; methanesulfonic acid; potassium tert-butylate; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; 1,2-dimethoxyethane; diethyl ether; hexane; dichloromethane; water;