C₃₆H₃₄ClFN₆O₇S₂

Base Information

Chemical Name:C₃₆H₃₄ClFN₆O₇S₂
CAS No.:1428146-21-7
Molecular Formula:C₃₆H₃₄ClFN₆O₇S₂
Molecular Weight:781.285
Hs Code.:

C<sub>36</sub>H<sub>34</sub>ClFN<sub>6</sub>O<sub>7</sub>S<sub>2</sub>

Synonyms:

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Chemical Property of C₃₆H₃₄ClFN₆O₇S₂

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Technology Process of C₃₆H₃₄ClFN₆O₇S₂

There total 9 articles about C₃₆H₃₄ClFN₆O₇S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1428146-03-5
5-(4-chlorophenyl)-1,2-dimethyl-N-(methylsulfonyl)-4-(3-(4-(4-nitrophenyl)piperazin-1-yl)phenyl)-1H-pyrrole-3-carboxamide

: 1428146-21-7
C₃₆H₃₄ClFN₆O₇S₂

Guidance literature:: Multi-step reaction with 2 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

2: pyridine / 0.5 h / 0 °C

With pyridine; palladium 10% on activated carbon; hydrogen; In methanol;
DOI:10.1021/jm4001105

Reference yield:

: 1384513-05-6
ethyl 2-acetyl-4-(4-chlorophenyl)-3-(3-iodophenyl)-4-oxobutanoate

: 1428146-21-7
C₃₆H₃₄ClFN₆O₇S₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: methanol / 24 h

1.2: 0.08 h

2.1: sodium hydroxide / water; ethanol; 1,4-dioxane / Reflux

3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / Reflux

4.1: dmap / 1,2-dichloro-ethane / Reflux

5.1: L-proline; copper(l) iodide / dimethyl sulfoxide / Inert atmosphere; Heating

6.1: palladium 10% on activated carbon; hydrogen / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

7.1: pyridine / 0.5 h / 0 °C

With pyridine; dmap; copper(l) iodide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; N,N-dimethyl-formamide; L-proline; sodium hydroxide; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; 1.2: |Paal-Knorr Pyrrole Synthesis / 5.1: |Ullmann Condensation;
DOI:10.1021/jm4001105

Reference yield:

: 1384513-06-7
ethyl 5-(4-chlorophenyl)-4-(3-iodophenyl)-1,2-dimethyl-1H-pyrrole-3-carboxylate

: 1428146-21-7
C₃₆H₃₄ClFN₆O₇S₂

Guidance literature:: Multi-step reaction with 6 steps

1: sodium hydroxide / water; ethanol; 1,4-dioxane / Reflux

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / Reflux

3: dmap / 1,2-dichloro-ethane / Reflux

4: L-proline; copper(l) iodide / dimethyl sulfoxide / Inert atmosphere; Heating

5: palladium 10% on activated carbon; hydrogen / methanol / 0.25 h / 760.05 Torr / Inert atmosphere

6: pyridine / 0.5 h / 0 °C

With pyridine; dmap; copper(l) iodide; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; N,N-dimethyl-formamide; L-proline; sodium hydroxide; In 1,4-dioxane; methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; 1,2-dichloro-ethane; 4: |Ullmann Condensation;
DOI:10.1021/jm4001105