(2-(2-(diphenylphosphino)phenyl)-4-methyl-4,5-dihydrooxazole)-(η4-1,5-cyclooctadiene)iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Base Information

Chemical Name:(2-(2-(diphenylphosphino)phenyl)-4-methyl-4,5-dihydrooxazole)-(η4-1,5-cyclooctadiene)iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate
CAS No.:1228538-88-2
Molecular Formula:C₃₀H₃₂IrNOP*C₃₂H₁₂BF₂₄
Molecular Weight:1509
Hs Code.:

(2-(2-(diphenylphosphino)phenyl)-4-methyl-4,5-dihydrooxazole)-(η4-1,5-cyclooctadiene)iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

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Chemical Property of (2-(2-(diphenylphosphino)phenyl)-4-methyl-4,5-dihydrooxazole)-(η4-1,5-cyclooctadiene)iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

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Technology Process of (2-(2-(diphenylphosphino)phenyl)-4-methyl-4,5-dihydrooxazole)-(η4-1,5-cyclooctadiene)iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

There total 1 articles about (2-(2-(diphenylphosphino)phenyl)-4-methyl-4,5-dihydrooxazole)-(η4-1,5-cyclooctadiene)iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 12112-67-3
bis(1,5-cyclooctadiene)diiridium(I) dichloride

: 1228312-87-5
2-(2-fluorophenyl)-4-methyl-4,5-dihydrooxazole

: 79060-88-1
sodium tetrakis[(3,5-di-trifluoromethyl)phenyl]borate

: 829-85-6
diphenylphosphane

: 1228538-88-2
(2-(2-(diphenylphosphino)phenyl)-4-methyl-4,5-dihydrooxazole)-(η4-1,5-cyclooctadiene)iridium(I) tetrakis(3,5-bis(trifluoromethyl)phenyl)borate

Guidance literature:: With n-butyllithium; In dichloromethane; (N2); N-BuLi in hexane added to Et2O soln. of phosphine deriv. at room temp.; stirred for 5 min; oxazoline deriv. added; stirred overnight; evapn.; CH2Cl2 soln. of (Ir(COD)Cl)2 added; refluxed for 2 h; cooled; (air); borate deriv. added at room temp.; stirred for 1-3 h; silica gel added; vac. evapn. at room temp.; silica placed on top of a column; chromy. (silica, CH2Cl2); vac. evapn.; vac. dried; detn. by NMR, MS;
DOI:10.1515/znb-2009-1007