Technology Process of C76H116N6O4Pd
There total 5 articles about C76H116N6O4Pd which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydride;
In
dichloromethane;
for 24h;
Inert atmosphere;
Reflux;
DOI:10.1039/c4dt00369a
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: potassium carbonate; potassium iodide / acetone
2.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C
2.2: 24 h / Reflux
3.1: hydrazine hydrate / ethanol / 24 h / 80 °C
4.1: sodium hydride / dichloromethane / 24 h / Inert atmosphere; Reflux
With
sodium hydride; potassium carbonate; hydrazine hydrate; potassium iodide;
In
tetrahydrofuran; ethanol; dichloromethane; acetone;
DOI:10.1039/c4dt00369a
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran / 1 h / 20 °C
1.2: 24 h / Reflux
2.1: hydrazine hydrate / ethanol / 24 h / 80 °C
3.1: sodium hydride / dichloromethane / 24 h / Inert atmosphere; Reflux
With
sodium hydride; hydrazine hydrate;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1039/c4dt00369a