Formic acid (S)-1-((S)-5-allyloxycarbonylamino-2-{(5S,10S)-10-[(S)-1-azido-2-(4-benzyloxy-phenyl)-ethyl]-5-isobutyl-3,6-dioxo-[1,4,7]oxadiazecan-7-yl}-pentanoyl)-pyrrolidin-2-ylmethyl ester

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Chemical Name:Formic acid (S)-1-((S)-5-allyloxycarbonylamino-2-{(5S,10S)-10-[(S)-1-azido-2-(4-benzyloxy-phenyl)-ethyl]-5-isobutyl-3,6-dioxo-[1,4,7]oxadiazecan-7-yl}-pentanoyl)-pyrrolidin-2-ylmethyl ester
CAS No.:854443-34-8
Molecular Formula:C₄₁H₅₅N₇O₉
Molecular Weight:789.929
Hs Code.:

Formic acid (S)-1-((S)-5-allyloxycarbonylamino-2-{(5S,10S)-10-[(S)-1-azido-2-(4-benzyloxy-phenyl)-ethyl]-5-isobutyl-3,6-dioxo-[1,4,7]oxadiazecan-7-yl}-pentanoyl)-pyrrolidin-2-ylmethyl ester

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Chemical Property of Formic acid (S)-1-((S)-5-allyloxycarbonylamino-2-{(5S,10S)-10-[(S)-1-azido-2-(4-benzyloxy-phenyl)-ethyl]-5-isobutyl-3,6-dioxo-[1,4,7]oxadiazecan-7-yl}-pentanoyl)-pyrrolidin-2-ylmethyl ester

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Technology Process of Formic acid (S)-1-((S)-5-allyloxycarbonylamino-2-{(5S,10S)-10-[(S)-1-azido-2-(4-benzyloxy-phenyl)-ethyl]-5-isobutyl-3,6-dioxo-[1,4,7]oxadiazecan-7-yl}-pentanoyl)-pyrrolidin-2-ylmethyl ester

There total 2 articles about Formic acid (S)-1-((S)-5-allyloxycarbonylamino-2-{(5S,10S)-10-[(S)-1-azido-2-(4-benzyloxy-phenyl)-ethyl]-5-isobutyl-3,6-dioxo-[1,4,7]oxadiazecan-7-yl}-pentanoyl)-pyrrolidin-2-ylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 854443-33-7
[(1S,2S)-1-(2-{[(S)-4-Allyloxycarbonylamino-1-((S)-2-formyloxymethyl-pyrrolidine-1-carbonyl)-butyl]-[(S)-2-(9H-fluoren-9-ylmethoxycarbonylamino)-4-methyl-pentanoyl]-amino}-ethyl)-2-azido-3-(4-benzyloxy-phenyl)-propoxy]-acetic acid

: 854443-34-8
Formic acid (S)-1-((S)-5-allyloxycarbonylamino-2-{(5S,10S)-10-[(S)-1-azido-2-(4-benzyloxy-phenyl)-ethyl]-5-isobutyl-3,6-dioxo-[1,4,7]oxadiazecan-7-yl}-pentanoyl)-pyrrolidin-2-ylmethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 115 mg / 2-dimethylaminoisopropyl chloride hydrochloride / ethyl acetate / 1 h / 0 °C

2: 39 mg / 1,8-diazabicyclo[5.4.0]undec-7-ene / dioxane / 3.5 h / Heating

With (2-chloropropyl)dimethylamine hydrochloride; 1,8-diazabicyclo[5.4.0]undec-7-ene; In 1,4-dioxane; ethyl acetate;
DOI:10.1016/j.tet.2005.03.061