C₃₁H₄₄N₄O₅SSi

Base Information

Chemical Name:C₃₁H₄₄N₄O₅SSi
CAS No.:1355952-08-7
Molecular Formula:C₃₁H₄₄N₄O₅SSi
Molecular Weight:612.866
Hs Code.:

C<sub>31</sub>H<sub>44</sub>N<sub>4</sub>O<sub>5</sub>SSi

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₁H₄₄N₄O₅SSi

Chemical Property:

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Technology Process of C₃₁H₄₄N₄O₅SSi

There total 9 articles about C₃₁H₄₄N₄O₅SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1355952-06-5
C₂₈H₄₀N₄O₅SSi

: 77-76-9
2,2-dimethoxy-propane

: 1355952-08-7
C₃₁H₄₄N₄O₅SSi

Guidance literature:: With toluene-4-sulfonic acid; at 20 ℃; for 3h;
DOI:10.1002/anie.201106205

Reference yield:

: 202753-56-8
2-(1H-4-bromoindol-3-yl)-ethanol

: 1355952-08-7
C₃₁H₄₄N₄O₅SSi

Guidance literature:: Multi-step reaction with 7 steps

1.1: dmap; triethylamine / dichloromethane / 10 h / 0 - 20 °C

2.1: tetrabutylammomium bromide; sodium hydroxide / dichloromethane; water / 0.17 h / 20 °C

2.2: 0.67 h / 20 °C

3.1: tetrabutylammomium bromide; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine / N,N-dimethyl-formamide / 2 h / 100 °C / Inert atmosphere

4.1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

5.1: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

6.1: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

7.1: toluene-4-sulfonic acid / 3 h / 20 °C

With dmap; thionyl chloride; sodium azide; methanesulfonamide; tetrabutylammomium bromide; palladium diacetate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; tris-(o-tolyl)phosphine; sodium hydroxide; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 3.1: Heck reaction / 4.1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205

Reference yield:

: 1355951-99-3
C₂₈H₃₉NO₄SSi

: 1355952-08-7
C₃₁H₄₄N₄O₅SSi

Guidance literature:: Multi-step reaction with 4 steps

1: methanesulfonamide / water; tert-butyl alcohol / 240 h / 20 °C

2: thionyl chloride; triethylamine / dichloromethane / 0.5 h / 0 °C

3: sodium azide; tetrabutylammomium bromide / N,N-dimethyl-formamide / 19 h / 90 °C

4: toluene-4-sulfonic acid / 3 h / 20 °C

With thionyl chloride; sodium azide; methanesulfonamide; tetrabutylammomium bromide; toluene-4-sulfonic acid; triethylamine; In dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol; 1: Sharpless dihydroxylation;
DOI:10.1002/anie.201106205