Technology Process of C38H48N2O8
There total 7 articles about C38H48N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 8 steps
1: 82 percent / LiAlH4 / diethyl ether
2: 87 percent / p-toluenesulfonic acid / acetone
3: 82 percent / DCC, DMAP
4: 64 percent / Tebbe's reagent / toluene
5: 46 percent / toluene / 120 °C
6: DDQ
7: NaBH4 / methanol
8: 1.) thiocarbonyl diimidazole, DMAP, 2.) n-Bu3SnH, AIBN / 2.) toluene
With
dmap; sodium tetrahydroborate; lithium aluminium tetrahydride; Tebbe's reagent; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; toluene-4-sulfonic acid; di(1H-imidazol-2-yl)methanethione; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
methanol; diethyl ether; acetone; toluene;
DOI:10.1021/jo00048a005
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 87 percent / p-toluenesulfonic acid / acetone
2: 82 percent / DCC, DMAP
3: 64 percent / Tebbe's reagent / toluene
4: 46 percent / toluene / 120 °C
5: DDQ
6: NaBH4 / methanol
7: 1.) thiocarbonyl diimidazole, DMAP, 2.) n-Bu3SnH, AIBN / 2.) toluene
With
dmap; sodium tetrahydroborate; Tebbe's reagent; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; toluene-4-sulfonic acid; di(1H-imidazol-2-yl)methanethione; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
methanol; acetone; toluene;
DOI:10.1021/jo00048a005
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 46 percent / toluene / 120 °C
2: DDQ
3: NaBH4 / methanol
4: 1.) thiocarbonyl diimidazole, DMAP, 2.) n-Bu3SnH, AIBN / 2.) toluene
With
dmap; sodium tetrahydroborate; 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; di(1H-imidazol-2-yl)methanethione; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
methanol; toluene;
DOI:10.1021/jo00048a005