2,3,5-TRI-O-BENZYL-D-RIBOFURANOSE

Base Information

• Chemical Name: 2,3,5-TRI-O-BENZYL-D-RIBOFURANOSE
• CAS No.: 89615-45-2
• Molecular Formula: C₂₆H₂₈O₅
• Molecular Weight: 420.505
• Mol file: 89615-45-2.mol

Synonyms:2,3,5-TRI-O-BENZYL-D-RIBOFURANOSE;TRI-O-BENZYL-D-RIBOFURANOSE;2,3,5-Tri-O-benzyl-alpha-D-ribofuranose

Chemical Property of 2,3,5-TRI-O-BENZYL-D-RIBOFURANOSE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 54-55°C
• Flash Point: 298.856°C
• Density: 1.21
• Storage Temp.: -20°C Freezer
• Solubility.: Chloroform, Ethyl Acetate

Purity/Quality:

99%, ^*data from raw suppliers

2,3,5-Tri-O-benzyl-D-ribofuranose ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2,3,5-Tri-O-benzyl-D-ribofuranose (cas# 89615-45-2) is a compound useful in organic synthesis.

Technology Process of 2,3,5-TRI-O-BENZYL-D-RIBOFURANOSE

There total 48 articles about 2,3,5-TRI-O-BENZYL-D-RIBOFURANOSE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

2,3,5-tri-O-benzyl-1-O-methyl-D-xylofuranoside (197716-38-4) → 2,3,5-tri-O-benzyl-D-xylofuranose (16838-89-4,17073-88-0,60933-68-8,60933-69-9,73068-66-3,89361-52-4,89615-42-9,89615-45-2,96192-07-3)

Guidance literature:

With acetic acid; at 100 ℃;

DOI:10.1055/s-1998-1617

Reference yield: 85.0%

2,3,5-tri-O-benzyl-1-O-methyl-β-D-xylofuranoside (79083-41-3) → 2,3,5-tri-O-benzyl-D-xylofuranose (16838-89-4,17073-88-0,60933-68-8,60933-69-9,73068-66-3,89361-52-4,89615-42-9,89615-45-2,96192-07-3)

Guidance literature:

With trityl tetrafluoroborate; In dichloromethane; at 20 ℃; for 0.5h;

DOI:10.1021/jo800693w

Reference yield: 78.0%

methyl-2,3,5-tri-O-benzyl-D-lyxofuranoside (302800-57-3) → 2,3,5-tri-O-benzyl-D-lyxofuranoside (16838-89-4,17073-88-0,60933-68-8,60933-69-9,73068-66-3,89361-52-4,89615-42-9,89615-45-2,96192-07-3)

Guidance literature:

With sulfuric acid; acetic acid; In water; at 100 ℃; for 0.5h; Inert atmosphere;

DOI:10.1002/ejoc.201601639

upstream raw materials:

methyl 2,3,5-tri-O-benzyl-α-L-ribofuranoside

benzyl bromide

(2S,3R,4S)-2-(hydroxymethyl)-5-methoxyoxolane-3,4-diol

methyl α-L-ribofuranoside

Downstream raw materials:

1,3,4-tri-O-benzyl-D-ribitol

2-[(1S,2R,3S,4S)-2,3,5-tris(benzyloxy)-1,4-dihydroxypent-1-yl]-N-triphenylmethylimidazole

2-[(1R,2R,3S,4S)-2,3,5-tris(benzyloxy)-1,4-dihydroxypent-1-yl]-N-triphenylmethylimidazole

(1S,2R,3S,4S)-2,3,5-Tris-benzyloxy-1-(2-trityl-2H-[1,2,4]triazol-3-yl)-pentane-1,4-diol

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