Technology Process of C26H34ClN5O5
There total 7 articles about C26H34ClN5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrazine hydrate / methanol / 12 h / 80 °C
2: tetrahydrofuran / 0.5 h / 60 °C
3: tin(II) chloride hydrate; hydrogenchloride / water; ethanol; ethyl acetate / 3 h / Reflux
4: dmap / tetrahydrofuran / 2 h
5: sodium cyanoborohydride; zinc(II) chloride; hydrogenchloride / water; methanol / 12 h
With
hydrogenchloride; dmap; tin(II) chloride hydrate; sodium cyanoborohydride; hydrazine hydrate; zinc(II) chloride;
In
tetrahydrofuran; methanol; ethanol; water; ethyl acetate;
DOI:10.1016/j.bmcl.2013.03.119
- Guidance literature:
-
Multi-step reaction with 4 steps
1: tetrahydrofuran / 0.5 h / 60 °C
2: tin(II) chloride hydrate; hydrogenchloride / water; ethanol; ethyl acetate / 3 h / Reflux
3: dmap / tetrahydrofuran / 2 h
4: sodium cyanoborohydride; zinc(II) chloride; hydrogenchloride / water; methanol / 12 h
With
hydrogenchloride; dmap; tin(II) chloride hydrate; sodium cyanoborohydride; zinc(II) chloride;
In
tetrahydrofuran; methanol; ethanol; water; ethyl acetate;
DOI:10.1016/j.bmcl.2013.03.119
- Guidance literature:
-
Multi-step reaction with 7 steps
1: sulfuric acid; nitric acid / water / 18 h / 60 °C
2: thionyl chloride / N,N-dimethyl-formamide / 3 h / 110 °C
3: hydrazine hydrate / methanol / 12 h / 80 °C
4: tetrahydrofuran / 0.5 h / 60 °C
5: tin(II) chloride hydrate; hydrogenchloride / water; ethanol; ethyl acetate / 3 h / Reflux
6: dmap / tetrahydrofuran / 2 h
7: sodium cyanoborohydride; zinc(II) chloride; hydrogenchloride / water; methanol / 12 h
With
hydrogenchloride; dmap; thionyl chloride; tin(II) chloride hydrate; sulfuric acid; nitric acid; sodium cyanoborohydride; hydrazine hydrate; zinc(II) chloride;
In
tetrahydrofuran; methanol; ethanol; water; ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2013.03.119