(2-phenyl-4,5,6,7-tetrahydroindenyl)(2-cyclohexylindenyl)zirconium dibromide

Base Information

Chemical Name:(2-phenyl-4,5,6,7-tetrahydroindenyl)(2-cyclohexylindenyl)zirconium dibromide
CAS No.:201803-91-0
Molecular Formula:C₃₀H₃₂Br₂Zr
Molecular Weight:643.616
Hs Code.:

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Chemical Property of (2-phenyl-4,5,6,7-tetrahydroindenyl)(2-cyclohexylindenyl)zirconium dibromide

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Technology Process of (2-phenyl-4,5,6,7-tetrahydroindenyl)(2-cyclohexylindenyl)zirconium dibromide

There total 1 articles about (2-phenyl-4,5,6,7-tetrahydroindenyl)(2-cyclohexylindenyl)zirconium dibromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19756-04-8
tetrakis(dimethylamido)zirconium (IV)

: 2857-97-8
trimethylsilyl bromide

: 156722-77-9
2-phenyl-4,5,6,7-tetrahydro-1H-indene

: 2-cyclohexylindene

: 201803-91-0
(2-phenyl-4,5,6,7-tetrahydroindenyl)(2-cyclohexylindenyl)zirconium dibromide

Guidance literature:: With BuLi (hexane); In hexane; toluene; byproducts: dimethylamine; inert atmosphere; stirring Zr(NMe2)4 and Ph-tetrahydroindene (MePh, 1 h,room temp.), evapn., dissoln. (MePh), cooling (0°C), addn. of Me 3SiBr, warming (room temp.), stirring (30 min), filtration, addn. to Li-salt of Cy-indene (-78°C); stirring for 6 h at room temp., filtration, extn. (hot MePh), evapn., washing (pentane), dissoln. (MePh), filtration (Celite), crystn. at -30°C; elem. anal.;
DOI:10.1021/om9706119